(C₄H₉)4N⁽¹⁺⁾*TcO₂(OC₆H₄CHNC₆H₄S)H₂O^(1-)=(C₄H₉)4N[TcO₂(OC₆H₄CHNC₆H₄S)(H₂O)]

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Chemical Name:(C₄H₉)4N⁽¹⁺⁾*TcO₂(OC₆H₄CHNC₆H₄S)H₂O^(1-)=(C₄H₉)4N[TcO₂(OC₆H₄CHNC₆H₄S)(H₂O)]
CAS No.:89554-16-5
Molecular Formula:C₁₃H₁₁NO₄STc*C₁₆H₃₆N
Molecular Weight:617.676
Hs Code.:

(C<sub>4</sub>H<sub>9</sub>)4N<sup>(1+)</sup>*TcO<sub>2</sub>(OC<sub>6</sub>H<sub>4</sub>CHNC<sub>6</sub>H<sub>4</sub>S)H<sub>2</sub>O<sup>(1-)</sup>=(C<sub>4</sub>H<sub>9</sub>)4N[TcO<sub>2</sub>(OC<sub>6</sub>H<sub>4</sub>CHNC<sub>6</sub>H<sub>4</sub>S)(H<sub>2</sub>O)]

Synonyms:(C₄H₉)4N⁽¹⁺⁾*TcO₂(OC₆H₄CHNC₆H₄S)H₂O^(1-)=(C₄H₉)4N[TcO₂(OC₆H₄CHNC₆H₄S)(H₂O)]

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Chemical Property of (C₄H₉)4N⁽¹⁺⁾*TcO₂(OC₆H₄CHNC₆H₄S)H₂O^(1-)=(C₄H₉)4N[TcO₂(OC₆H₄CHNC₆H₄S)(H₂O)]

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Technology Process of (C₄H₉)4N⁽¹⁺⁾*TcO₂(OC₆H₄CHNC₆H₄S)H₂O^(1-)=(C₄H₉)4N[TcO₂(OC₆H₄CHNC₆H₄S)(H₂O)]

There total 1 articles about (C₄H₉)4N⁽¹⁺⁾*TcO₂(OC₆H₄CHNC₆H₄S)H₂O^(1-)=(C₄H₉)4N[TcO₂(OC₆H₄CHNC₆H₄S)(H₂O)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: sodium dithionite

: 34035-97-7
ammonium pertechnetate

: 1112-67-0
tetrabutyl-ammonium chloride

: 3449-05-6
2-(salicylideneamino)thiophenol

: 89554-16-5
(C₄H₉)4N⁽¹⁺⁾*TcO₂(OC₆H₄CHNC₆H₄S)H₂O^(1-)=(C₄H₉)4N[TcO₂(OC₆H₄CHNC₆H₄S)(H₂O)]

Guidance literature:: With sodium hydroxide; In sodium hydroxide; addn. of NH4TcO4 to soln. of ligand in aq. NaOH, addn. of Na2S2O4 in aq. NaOH, addn. of 30% aq. Bu4NCl, stirring (5 min, pptn.); filtration, washing (NaOH, H2O), extn. (acetone), addn. of H2O, crystn.(-15°C, 24 h), filtration, washing (H2O), drying (vac., overnight); elem. anal.;
DOI:10.1016/S0020-1693(00)82492-5