Salicylideneamino-2-thiophenol

Base Information

• Chemical Name: Salicylideneamino-2-thiophenol
• CAS No.: 3449-05-6
• Molecular Formula: C13H11NOS
• Molecular Weight: 229.302
• Hs Code.: 2930909090
• European Community (EC) Number: 222-370-4
• Nikkaji Number: J7.737B,J3.125.321G,J3.085.641D
• Mol file: 3449-05-6.mol

Synonyms:salicylideneamino-2-thiophenol

Chemical Property of Salicylideneamino-2-thiophenol

Chemical Property:

• Vapor Pressure: 6.64E-08mmHg at 25°C
• Boiling Point: 438.9°Cat760mmHg
• Flash Point: 219.3°C
• PSA: 71.39000
• Density: 1.295g/cm³
• LogP: 3.43150
• Storage Temp.: Refrigerator
• XLogP3: 3.2
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 229.05613515
• Heavy Atom Count: 16
• Complexity: 244

Purity/Quality:

97% ^*data from raw suppliers

2-(SALICYLIDENEAMINO)THIOPHENOL AldrichCPR ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)C=NC2=CC=CC=C2S)O

Technology Process of Salicylideneamino-2-thiophenol

There total 114 articles about Salicylideneamino-2-thiophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

triphenylborane (1095-03-0) + hydrogen (1333-74-0) + trimethylamine (75-50-3) → trimethylamine-borane (75-22-9)

Guidance literature:

With aluminium; aluminium trichloride; In neat (no solvent); in presence of activated Al-powder, H2-pressure 2000 psi, 180°C, 1h;; separation by distn. in vac.;;

Reference yield: 98.0%

(CH3O)(CH3)2N*BH3 (127088-51-1) + trimethylamine (75-50-3) → trimethylamine-borane (75-22-9)

Guidance literature:

In diethyl ether; at 0°C;;

DOI:10.1021/ja01541a022

Reference yield: 92.5%

(CH3)3NGeH3Br (60342-06-5) + diborane (19287-45-7) → bromogermanate (13569-43-2) + trimethylamine-borane (75-22-9)

Guidance literature:

In neat (no solvent); byproducts: germanes; under N2 or in vac., excess B2H6, -78°C, 1.0 h;

DOI:10.1016/S0020-1693(00)85155-5

upstream raw materials:

2-methyl-benzyl alcohol

2-amino-benzenethiol

salicylaldehyde

salicylic alcohol

Downstream raw materials:

La⁽³⁺⁾*C₁₃H₉NOS^(2-)*(CH₃)3SiO^(1-)=La(C₁₃H₉NOS)OSi(CH₃)3

bis(3-methyl-1-phenyl-3-pyrazoline-5-one)(2-hydroxybenzalidene-aminothiophenolato)(H₂O)copper(II)

(C₄H₉)4N⁽¹⁺⁾*TcO₂(OC₆H₄CHNC₆H₄S)H₂O^(1-)=(C₄H₉)4N[TcO₂(OC₆H₄CHNC₆H₄S)(H₂O)]

(C₆H₁₁OCOCH₂CH₂)Sn(Cl)(SC₆H₄NCHC₆H₄O)

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