trans-1,4-dimethoxy-2,3,5-trimethyl-6-(3',7',11',15'-tetramethyl-2',6',10',14'-hexadecatetraenyl)benzene

Base Information

Chemical Name:trans-1,4-dimethoxy-2,3,5-trimethyl-6-(3',7',11',15'-tetramethyl-2',6',10',14'-hexadecatetraenyl)benzene
CAS No.:66958-65-4
Molecular Formula:C₃₁H₄₈O₂
Molecular Weight:452.721
Hs Code.:

Synonyms:trans-1,4-dimethoxy-2,3,5-trimethyl-6-(3',7',11',15'-tetramethyl-2',6',10',14'-hexadecatetraenyl)benzene

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Chemical Property of trans-1,4-dimethoxy-2,3,5-trimethyl-6-(3',7',11',15'-tetramethyl-2',6',10',14'-hexadecatetraenyl)benzene

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Technology Process of trans-1,4-dimethoxy-2,3,5-trimethyl-6-(3',7',11',15'-tetramethyl-2',6',10',14'-hexadecatetraenyl)benzene

There total 5 articles about trans-1,4-dimethoxy-2,3,5-trimethyl-6-(3',7',11',15'-tetramethyl-2',6',10',14'-hexadecatetraenyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: trans-1,4-dimethoxy-2,3,5-trimethyl-6-[3',7',11',15'-tetramethyl-9'-(p-toluenesulfonyl)-2',6',10',14'-hexadecatetraenyl]benzene

: 66958-65-4
trans-1,4-dimethoxy-2,3,5-trimethyl-6-(3',7',11',15'-tetramethyl-2',6',10',14'-hexadecatetraenyl)benzene

Guidance literature:

Reference yield:

: 66958-61-0
trans-1,4-dimethoxy-2,3,5-trimethyl-6-(3',7'-dimethyl-6'-hydroxy-2',7'-octadienyl)benzene

: 66958-65-4
trans-1,4-dimethoxy-2,3,5-trimethyl-6-(3',7',11',15'-tetramethyl-2',6',10',14'-hexadecatetraenyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / tetrahydrofuran

2: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane

3: lithium; ethylamine

With n-butyllithium; thionyl chloride; lithium; ethylamine; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane;

Reference yield:

: 66958-60-9
3-[(E)-5-(2,5-Dimethoxy-3,4,6-trimethyl-phenyl)-3-methyl-pent-3-enyl]-2,2-dimethyl-oxirane

: 66958-65-4
trans-1,4-dimethoxy-2,3,5-trimethyl-6-(3',7',11',15'-tetramethyl-2',6',10',14'-hexadecatetraenyl)benzene

Guidance literature:: Multi-step reaction with 4 steps

1: lithium diisopropyl amide / tetrahydrofuran

2: thionyl chloride / tetrahydrofuran

3: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane

4: lithium; ethylamine

With n-butyllithium; thionyl chloride; lithium; ethylamine; lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane;