3-(2-{2-[2-(3-hydroxy-3,3-diphenyl-prop-1-ynyl)-phenylethynyl]-phenylethynyl}-phenyl)-1,1-diphenyl-prop-2-yn-1-ol

Base Information

• Chemical Name: 3-(2-{2-[2-(3-hydroxy-3,3-diphenyl-prop-1-ynyl)-phenylethynyl]-phenylethynyl}-phenyl)-1,1-diphenyl-prop-2-yn-1-ol
• CAS No.: 874097-29-7
• Molecular Formula: C₅₂H₃₄O₂
• Molecular Weight: 690.841

Synonyms:3-(2-{2-[2-(3-hydroxy-3,3-diphenyl-prop-1-ynyl)-phenylethynyl]-phenylethynyl}-phenyl)-1,1-diphenyl-prop-2-yn-1-ol

Chemical Property of 3-(2-{2-[2-(3-hydroxy-3,3-diphenyl-prop-1-ynyl)-phenylethynyl]-phenylethynyl}-phenyl)-1,1-diphenyl-prop-2-yn-1-ol

Chemical Property:

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Technology Process of 3-(2-{2-[2-(3-hydroxy-3,3-diphenyl-prop-1-ynyl)-phenylethynyl]-phenylethynyl}-phenyl)-1,1-diphenyl-prop-2-yn-1-ol

There total 1 articles about 3-(2-{2-[2-(3-hydroxy-3,3-diphenyl-prop-1-ynyl)-phenylethynyl]-phenylethynyl}-phenyl)-1,1-diphenyl-prop-2-yn-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-bis[(2-ethynylphenyl)ethynyl]benzene + benzophenone (119-61-9) → 3-(2-{2-[2-(3-hydroxy-3,3-diphenyl-prop-1-ynyl)-phenylethynyl]-phenylethynyl}-phenyl)-1,1-diphenyl-prop-2-yn-1-ol (874097-29-7)

Guidance literature:

1,2-bis[(2-ethynylphenyl)ethynyl]benzene; With n-butyllithium; In diethyl ether; hexane; at 0 ℃; for 0.5h;

benzophenone; In diethyl ether; hexane; at 0 - 20 ℃;

DOI:10.1016/j.tet.2005.10.062

Reference yield: 83.0%

3-(2-{2-[2-(3-hydroxy-3,3-diphenyl-prop-1-ynyl)-phenylethynyl]-phenylethynyl}-phenyl)-1,1-diphenyl-prop-2-yn-1-ol (874097-29-7) → C52H34 (874097-33-3)

Guidance literature:

With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.0833333h;

DOI:10.1016/j.tet.2005.10.062

Reference yield:

3-(2-{2-[2-(3-hydroxy-3,3-diphenyl-prop-1-ynyl)-phenylethynyl]-phenylethynyl}-phenyl)-1,1-diphenyl-prop-2-yn-1-ol (874097-29-7) → C52H32Cl2

Guidance literature:

With pyridine; thionyl chloride; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1016/j.tet.2005.10.062

upstream raw materials:

benzophenone

Downstream raw materials:

C₅₂H₃₄

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