2-O-<<(tert-butyldimethylsilyl)oxy>acetyl>-10-(dicyclohexylsulfamoyl)-D-isoborneol

Base Information

Chemical Name:2-O-<<(tert-butyldimethylsilyl)oxy>acetyl>-10-(dicyclohexylsulfamoyl)-D-isoborneol
CAS No.:132127-26-5
Molecular Formula:C₃₀H₅₅NO₅SSi
Molecular Weight:569.922
Hs Code.:

Synonyms:2-O-<<(tert-butyldimethylsilyl)oxy>acetyl>-10-(dicyclohexylsulfamoyl)-D-isoborneol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-O-<<(tert-butyldimethylsilyl)oxy>acetyl>-10-(dicyclohexylsulfamoyl)-D-isoborneol

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Technology Process of 2-O-<<(tert-butyldimethylsilyl)oxy>acetyl>-10-(dicyclohexylsulfamoyl)-D-isoborneol

There total 4 articles about 2-O-<<(tert-butyldimethylsilyl)oxy>acetyl>-10-(dicyclohexylsulfamoyl)-D-isoborneol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 175917-88-1
10-(dicyclohexylsulfamoyl)-2-O-(hydroxyacetyl)-D-isoborneol

: 132127-26-5
2-O-<<(tert-butyldimethylsilyl)oxy>acetyl>-10-(dicyclohexylsulfamoyl)-D-isoborneol

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1021/jo951961c

Reference yield:

: 96303-88-7
(-)-10-dicyclohexylsulfamoyl-D-isoborneol

: 132127-26-5
2-O-<<(tert-butyldimethylsilyl)oxy>acetyl>-10-(dicyclohexylsulfamoyl)-D-isoborneol

Guidance literature:: Multi-step reaction with 4 steps

1: DMAP / tetrahydrofuran / Heating

2: tetrabutylamonium bromide / toluene / 12 h / Heating

3: conc. HCl / methanol / 0.17 h

4: 98 percent / Et₃N, DMAP / CH₂Cl₂ / 2 h / Ambient temperature

With hydrogenchloride; dmap; tetrabutylammomium bromide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/jo951961c

Reference yield:

: 130156-92-2
2-O-(chloroacetyl)-10-(dicyclohexylsulfamoyl)-D-isoborneol

: 132127-26-5
2-O-<<(tert-butyldimethylsilyl)oxy>acetyl>-10-(dicyclohexylsulfamoyl)-D-isoborneol

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutylamonium bromide / toluene / 12 h / Heating

2: conc. HCl / methanol / 0.17 h

3: 98 percent / Et₃N, DMAP / CH₂Cl₂ / 2 h / Ambient temperature

With hydrogenchloride; dmap; tetrabutylammomium bromide; triethylamine; In methanol; dichloromethane; toluene;
DOI:10.1021/jo951961c