N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzenesulfenamide

Base Information

Chemical Name:N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzenesulfenamide
CAS No.:130485-95-9
Molecular Formula:C₁₇H₂₃NS
Molecular Weight:273.442
Hs Code.:

Synonyms:N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzenesulfenamide

Suppliers and Price of N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzenesulfenamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzenesulfenamide

Chemical Property:

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Technology Process of N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzenesulfenamide

There total 3 articles about N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzenesulfenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 17745-52-7
N,N-bis(trimethylsilyl)-phenylsulphenamide

: 127826-98-6
(+/-)-(1,5,5-trimethyl-2-cyclohexen-1-yl)acetaldehyde

: 130485-95-9
N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzenesulfenamide

Guidance literature:: tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/S0040-4020(01)80849-8

Reference yield:

: 470-99-5
isophorol

: 130485-95-9
N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzenesulfenamide

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / mercuric acetate , allyl alcohol / 24 h / 33 °C

2: 75 percent / 0.5 h / 215 °C

3: 89 percent / 1.1 M tetrabutylammonium fluoride / tetrahydrofuran / 20 °C

With mercury(II) diacetate; allyl alcohol; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)80849-8

Reference yield:

: 124938-43-8
3-(ethenyloxy)-1,5,5-trimethylcyclohexene

: 130485-95-9
N-<2-(1,5,5-trimethyl-2-cyclohexen-1-yl)ethylidene>-2-benzenesulfenamide

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / 0.5 h / 215 °C

2: 89 percent / 1.1 M tetrabutylammonium fluoride / tetrahydrofuran / 20 °C

tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)80849-8