Benzenesulfenamide, N,N-bis(trimethylsilyl)-

Base Information

Chemical Name:Benzenesulfenamide, N,N-bis(trimethylsilyl)-
CAS No.:17745-52-7
Molecular Formula:C12H23NSSi2
Molecular Weight:269.558
Hs Code.:
DSSTox Substance ID:DTXSID00474181
Wikidata:Q82304014

Synonyms:Benzenesulfenamide, N,N-bis(trimethylsilyl)-;17745-52-7;DTXSID00474181;N-phenylsulfenyl hexamethyldisilazane

Suppliers and Price of Benzenesulfenamide, N,N-bis(trimethylsilyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Benzenesulfenamide, N,N-bis(trimethylsilyl)-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:269.10897398
Heavy Atom Count:16
Complexity:200

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)N([Si](C)(C)C)SC1=CC=CC=C1

Technology Process of Benzenesulfenamide, N,N-bis(trimethylsilyl)-

There total 4 articles about Benzenesulfenamide, N,N-bis(trimethylsilyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 931-59-9
benzenesulfenyl chloride

: 4039-32-1
lithium hexamethyldisilazane

: 17745-52-7
N,N-bis(trimethylsilyl)-phenylsulphenamide

Guidance literature:: In diethyl ether;
DOI:10.1007/BF00954032

Reference yield:

: 75-46-7
trifluoromethan

: 882-33-7
diphenyldisulfane

: 4039-32-1
lithium hexamethyldisilazane

: 1535-67-7
difluoromethyl phenyl sulfide

: 17745-52-7
N,N-bis(trimethylsilyl)-phenylsulphenamide

: 456-56-4
phenyl trifluoromethylsulfide

Guidance literature:: With 1,1,1,3,3,3-hexamethyl-disilazane; In tetrahydrofuran; N,N-dimethyl-formamide; at -15 - 20 ℃; for 17.5h;
DOI:10.1021/jo000150s

Reference yield:

: 1212-08-4
S-Phenyl benzenethiosulfonate

: 105930-38-9
(4S,5E)-7-methylene-4-(1-methylethyl)-5-cyclodecene-1-one

: 17745-52-7
N,N-bis(trimethylsilyl)-phenylsulphenamide

: 90460-45-0,105371-09-3,113666-99-2
(4S,5E)-4-isopropyl-7-methylene-10-phenylthio-5-cyclodecen-1-one

Guidance literature:: With n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane; Multistep reaction; 1.) THF, n-hexane, -10 deg C, 10 min; 2.) THF, -70 deg C, 1 h; 3.) THF, -5 to 20 deg C, 5 min;
DOI:10.1016/S0040-4020(01)86874-5