(E)-4-(3-(3,5-dichloro-4-fluorophenyl)-4,4,4-trifluorobut-1-enyl)-2-(trifluoromethoxy)benzoic acid

Base Information Edit

Chemical Name:(E)-4-(3-(3,5-dichloro-4-fluorophenyl)-4,4,4-trifluorobut-1-enyl)-2-(trifluoromethoxy)benzoic acid
CAS No.:1416979-96-8
Molecular Formula:C₁₈H₉Cl₂F₇O₃
Molecular Weight:477.162
Hs Code.:
Mol file:1416979-96-8.mol

Synonyms:(E)-4-(3-(3,5-dichloro-4-fluorophenyl)-4,4,4-trifluorobut-1-enyl)-2-(trifluoromethoxy)benzoic acid

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Chemical Property of (E)-4-(3-(3,5-dichloro-4-fluorophenyl)-4,4,4-trifluorobut-1-enyl)-2-(trifluoromethoxy)benzoic acid Edit

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Technology Process of (E)-4-(3-(3,5-dichloro-4-fluorophenyl)-4,4,4-trifluorobut-1-enyl)-2-(trifluoromethoxy)benzoic acid

There total 3 articles about (E)-4-(3-(3,5-dichloro-4-fluorophenyl)-4,4,4-trifluorobut-1-enyl)-2-(trifluoromethoxy)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 1416979-95-7
2-(trifluoromethoxy)-4-vinylbenzoic acid

: 1416979-51-5
5-(1-bromo-2,2,2-trifluoroethyl)-1,3-dichloro-2-fluorobenzene

: 1416979-96-8
(E)-4-(3-(3,5-dichloro-4-fluorophenyl)-4,4,4-trifluorobut-1-enyl)-2-(trifluoromethoxy)benzoic acid

Guidance literature:: [2,2]bipyridinyl; copper(l) chloride; In 1-Methylpyrrolidine; at 150 ℃; for 1h;

Reference yield:

: 509142-48-7
4-bromo-2-(trifluoromethoxy)benzoic acid

: 1416979-96-8
(E)-4-(3-(3,5-dichloro-4-fluorophenyl)-4,4,4-trifluorobut-1-enyl)-2-(trifluoromethoxy)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 1 h / 80 °C / Inert atmosphere

2: [2,2]bipyridinyl; copper(l) chloride / 1-Methylpyrrolidine / 1 h / 150 °C

With potassium carbonate; [2,2]bipyridinyl; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) chloride; In 1-Methylpyrrolidine; dimethyl sulfoxide;