ethyl 2-(6-(4-((4-chlorobenzyl)oxy)-2-oxopyridin-1(2H)-yl)-3-methylimidazo[1,2-a]pyridin-2-yl)cyclopropanecarboxylate

Base Information

Chemical Name:ethyl 2-(6-(4-((4-chlorobenzyl)oxy)-2-oxopyridin-1(2H)-yl)-3-methylimidazo[1,2-a]pyridin-2-yl)cyclopropanecarboxylate
CAS No.:1447913-44-1
Molecular Formula:C₂₆H₂₄ClN₃O₄
Molecular Weight:477.947
Hs Code.:

Synonyms:ethyl 2-(6-(4-((4-chlorobenzyl)oxy)-2-oxopyridin-1(2H)-yl)-3-methylimidazo[1,2-a]pyridin-2-yl)cyclopropanecarboxylate

Suppliers and Price of ethyl 2-(6-(4-((4-chlorobenzyl)oxy)-2-oxopyridin-1(2H)-yl)-3-methylimidazo[1,2-a]pyridin-2-yl)cyclopropanecarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl 2-(6-(4-((4-chlorobenzyl)oxy)-2-oxopyridin-1(2H)-yl)-3-methylimidazo[1,2-a]pyridin-2-yl)cyclopropanecarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl 2-(6-(4-((4-chlorobenzyl)oxy)-2-oxopyridin-1(2H)-yl)-3-methylimidazo[1,2-a]pyridin-2-yl)cyclopropanecarboxylate

There total 4 articles about ethyl 2-(6-(4-((4-chlorobenzyl)oxy)-2-oxopyridin-1(2H)-yl)-3-methylimidazo[1,2-a]pyridin-2-yl)cyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1447913-43-0
ethyl 2-(6-iodo-3-methylimidazo[1,2-a]pyridin-2-yl)cyclopropanecarboxylate

: 191090-84-3
4-{[(4-chlorophenyl)methyl]oxy}-2(1H)-pyridinone

: 1447913-44-1
ethyl 2-(6-(4-((4-chlorobenzyl)oxy)-2-oxopyridin-1(2H)-yl)-3-methylimidazo[1,2-a]pyridin-2-yl)cyclopropanecarboxylate

Guidance literature:: With trans-N,N'-dimethyl-1,2-cyclohexyldiamine; copper(l) iodide; potassium carbonate; In 1,4-dioxane; at 110 ℃; for 12h;

Reference yield:

: 1447911-51-4
ethyl 6-iodo-3-methylimidazo[1,2-a]pyridine-2-carboxylic acid

: 1447913-44-1
ethyl 2-(6-(4-((4-chlorobenzyl)oxy)-2-oxopyridin-1(2H)-yl)-3-methylimidazo[1,2-a]pyridin-2-yl)cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: diisobutylaluminium hydride / dichloromethane; toluene / 2 h / -78 °C

2: sodium hydride / mineral oil; tetrahydrofuran / 0 - 20 °C

3: 5,5-dimethyl-1,3-cyclohexadiene / 5 h / Reflux

4: potassium carbonate; copper(l) iodide; trans-N,N'-dimethyl-1,2-cyclohexyldiamine / 1,4-dioxane / 12 h / 110 °C

With trans-N,N'-dimethyl-1,2-cyclohexyldiamine; copper(l) iodide; sodium hydride; diisobutylaluminium hydride; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; toluene; mineral oil;

Reference yield:

: 1447912-45-9
6-iodo-3-methylimidazo[1,2-a]pyridine-2-carbaldehyde

: 1447913-44-1
ethyl 2-(6-(4-((4-chlorobenzyl)oxy)-2-oxopyridin-1(2H)-yl)-3-methylimidazo[1,2-a]pyridin-2-yl)cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / mineral oil; tetrahydrofuran / 0 - 20 °C

2: 5,5-dimethyl-1,3-cyclohexadiene / 5 h / Reflux

3: potassium carbonate; copper(l) iodide; trans-N,N'-dimethyl-1,2-cyclohexyldiamine / 1,4-dioxane / 12 h / 110 °C

With trans-N,N'-dimethyl-1,2-cyclohexyldiamine; copper(l) iodide; sodium hydride; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; 5,5-dimethyl-1,3-cyclohexadiene; mineral oil;