Ethanone, 1-[3-(4-bromophenyl)-4,6-dimethoxy-2-methyl-1H-indol-7-yl]-2,2,2-trichloro-

Base Information

Chemical Name:Ethanone, 1-[3-(4-bromophenyl)-4,6-dimethoxy-2-methyl-1H-indol-7-yl]-2,2,2-trichloro-
CAS No.:869960-02-1
Molecular Formula:C19H15 Br Cl3 N O3
Molecular Weight:491.59
Hs Code.:
Mol file:869960-02-1.mol

Synonyms:Ethanone, 1-[3-(4-bromophenyl)-4,6-dimethoxy-2-methyl-1H-indol-7-yl]-2,2,2-trichloro-

Suppliers and Price of Ethanone, 1-[3-(4-bromophenyl)-4,6-dimethoxy-2-methyl-1H-indol-7-yl]-2,2,2-trichloro-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethanone, 1-[3-(4-bromophenyl)-4,6-dimethoxy-2-methyl-1H-indol-7-yl]-2,2,2-trichloro-

Chemical Property:

Melting Point:181 - 182 °C
PSA：51.32000
LogP:6.47590

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Ethanone, 1-[3-(4-bromophenyl)-4,6-dimethoxy-2-methyl-1H-indol-7-yl]-2,2,2-trichloro-

There total 6 articles about Ethanone, 1-[3-(4-bromophenyl)-4,6-dimethoxy-2-methyl-1H-indol-7-yl]-2,2,2-trichloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 76-02-8
trifluoroacetyl chloride

: 845548-60-9
3-(4-bromophenyl)-4,6-dimethoxy-2-methylindole

: 869960-02-1
3-(4-bromophenyl)-4,6-dimethoxy-2-methyl-7-trichloroacetylindole

Guidance literature:: In chloroform; Heating;
DOI:10.1016/j.tet.2005.08.048

Reference yield:

: 869959-91-1
1-(4-bromophenyl)-2-[(3,5-dimethoxyphenyl)amino] propanone

: 869960-02-1
3-(4-bromophenyl)-4,6-dimethoxy-2-methyl-7-trichloroacetylindole

Guidance literature:: Multi-step reaction with 4 steps

1.1: 50 °C

1.2: 92 percent / water

2.1: 77 percent / trifluoroacetic acid

3.1: 86 percent / potassium hydroxide / methanol

4.1: 85 percent / CHCl₃ / Heating

With potassium hydroxide; trifluoroacetic acid; In methanol; chloroform;
DOI:10.1016/j.tet.2005.08.048

Reference yield:

: 869960-21-4
N-acetyl-1-(4-bromophenyl)-2-[(3,5-dimethoxyphenyl)amido] prpanone

: 869960-02-1
3-(4-bromophenyl)-4,6-dimethoxy-2-methyl-7-trichloroacetylindole

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / trifluoroacetic acid

2: 86 percent / potassium hydroxide / methanol

3: 85 percent / CHCl₃ / Heating

With potassium hydroxide; trifluoroacetic acid; In methanol; chloroform;
DOI:10.1016/j.tet.2005.08.048