4-chloro-3-(N-chloro-N-(dichloro(4-methylphenyl)methyl)amino)butanenitrile

Base Information

Chemical Name:4-chloro-3-(N-chloro-N-(dichloro(4-methylphenyl)methyl)amino)butanenitrile
CAS No.:897440-44-7
Molecular Formula:C₁₂H₁₂Cl₄N₂
Molecular Weight:326.053
Hs Code.:

Synonyms:4-chloro-3-(N-chloro-N-(dichloro(4-methylphenyl)methyl)amino)butanenitrile

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Chemical Property of 4-chloro-3-(N-chloro-N-(dichloro(4-methylphenyl)methyl)amino)butanenitrile

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Technology Process of 4-chloro-3-(N-chloro-N-(dichloro(4-methylphenyl)methyl)amino)butanenitrile

There total 2 articles about 4-chloro-3-(N-chloro-N-(dichloro(4-methylphenyl)methyl)amino)butanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 897440-36-7
2-(cyanomethyl)-1-(4-methylbenzyl)aziridine

: 897440-44-7
4-chloro-3-(N-chloro-N-(dichloro(4-methylphenyl)methyl)amino)butanenitrile

Guidance literature:: With N-chloro-succinimide; dibenzoyl peroxide; In tetrachloromethane; for 40h; Heating;
DOI:10.1021/jo060425p

Reference yield:

: 156697-63-1
2-(bromomethyl)-1-<(4-methylphenyl)methyl>aziridine

: 897440-44-7
4-chloro-3-(N-chloro-N-(dichloro(4-methylphenyl)methyl)amino)butanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / dimethylsulfoxide / 3 h / 60 - 70 °C

2: 82 percent / NCS; benzoylperoxide / CCl₄ / 40 h / Heating

With N-chloro-succinimide; dibenzoyl peroxide; In tetrachloromethane; dimethyl sulfoxide;
DOI:10.1021/jo060425p