4-[3'-(4''-benzyloxyphenyl-1''-propyl)oxy]-3,5-dimethylnitrobenzene

Base Information

• Chemical Name: 4-[3'-(4''-benzyloxyphenyl-1''-propyl)oxy]-3,5-dimethylnitrobenzene
• CAS No.: 1029554-82-2
• Molecular Formula: C₂₄H₂₅NO₄
• Molecular Weight: 391.467
• Mol file: 1029554-82-2.mol

Synonyms:4-[3'-(4''-benzyloxyphenyl-1''-propyl)oxy]-3,5-dimethylnitrobenzene

Chemical Property of 4-[3'-(4''-benzyloxyphenyl-1''-propyl)oxy]-3,5-dimethylnitrobenzene

Chemical Property:

Purity/Quality:

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Technology Process of 4-[3'-(4''-benzyloxyphenyl-1''-propyl)oxy]-3,5-dimethylnitrobenzene

There total 1 articles about 4-[3'-(4''-benzyloxyphenyl-1''-propyl)oxy]-3,5-dimethylnitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2,6-dimethyl-4-nitro phenol (2423-71-4) + 3-[4-(benzyloxy)phenyl]propan-1-ol (61440-45-7) → 4-[3'-(4''-benzyloxyphenyl-1''-propyl)oxy]-3,5-dimethylnitrobenzene (1029554-82-2)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 25 ℃; for 19h;

DOI:10.1021/jo800094q

Reference yield: 51.0%

4-[3'-(4''-benzyloxyphenyl-1''-propyl)oxy]-3,5-dimethylnitrobenzene (1029554-82-2) → 4-[3'-(4''-benzyloxyphenyl-1''-propyl)oxy]-3,5-dimethylaniline (1029554-84-4)

Guidance literature:

With tin(ll) chloride; In tetrahydrofuran; ethanol; for 9h; Heating;

DOI:10.1021/jo800094q

upstream raw materials:

2,6-dimethyl-4-nitro phenol

3-[4-(benzyloxy)phenyl]propan-1-ol

Downstream raw materials:

4-[3'-(4''-benzyloxyphenyl-1''-propyl)oxy]-3,5-dimethylaniline