C₃₁H₃₅N₃O₉S₂

Base Information

Chemical Name:C₃₁H₃₅N₃O₉S₂
CAS No.:1355951-88-0
Molecular Formula:C₃₁H₃₅N₃O₉S₂
Molecular Weight:657.766
Hs Code.:

C<sub>31</sub>H<sub>35</sub>N<sub>3</sub>O<sub>9</sub>S<sub>2</sub>

Synonyms:C₃₁H₃₅N₃O₉S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₃₅N₃O₉S₂

Chemical Property:

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Technology Process of C₃₁H₃₅N₃O₉S₂

There total 11 articles about C₃₁H₃₅N₃O₉S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1355952-10-1
C₃₇H₄₉N₃O₉S₂Si

: 1355951-88-0
C₃₁H₃₅N₃O₉S₂

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 48h;
DOI:10.1002/anie.201106205

Reference yield:

: 202753-56-8
2-(1H-4-bromoindol-3-yl)-ethanol

: 1355951-88-0
C₃₁H₃₅N₃O₉S₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: dmap; triethylamine / dichloromethane / 10 h / 0 - 20 °C

2.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane; water / 0.17 h / 20 °C

2.2: 0.67 h / 20 °C

3.1: tetrabutylammomium bromide; palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

4.1: methanesulfonamide / water; tert-butyl alcohol / 240 h / 20 °C

5.1: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C

6.1: sodium azide; tetrabutylammomium bromide / N,N-dimethyl-formamide / 19 h / 90 °C

7.1: toluene-4-sulfonic acid / 3 h / 20 °C

8.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C

9.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 48 h / 20 °C

With dmap; lithium aluminium tetrahydride; thionyl chloride; sodium azide; methanesulfonamide; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; palladium diacetate; potassium carbonate; toluene-4-sulfonic acid; triethylamine; tris-(o-tolyl)phosphine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 3.1: Heck reaction / 4.1: Sharpless dihydroxylation;
DOI:10.1002/anie.201106205

Reference yield:

: 1355951-99-3
C₂₈H₃₉NO₄SSi

: 1355951-88-0
C₃₁H₃₅N₃O₉S₂

Guidance literature:: Multi-step reaction with 7 steps

1: methanesulfonamide / water; tert-butyl alcohol / 240 h / 20 °C

2: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C

3: sodium azide; tetrabutylammomium bromide / N,N-dimethyl-formamide / 19 h / 90 °C

4: toluene-4-sulfonic acid / 3 h / 20 °C

5: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C

6: dmap; triethylamine / dichloromethane / 12 h / 20 °C

7: tetrabutyl ammonium fluoride / tetrahydrofuran / 48 h / 20 °C

With dmap; lithium aluminium tetrahydride; thionyl chloride; sodium azide; methanesulfonamide; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1: Sharpless dihydroxylation;
DOI:10.1002/anie.201106205