C₂₃H₃₃N₂OPS

Base Information

Chemical Name:C₂₃H₃₃N₂OPS
CAS No.:952301-65-4
Molecular Formula:C₂₃H₃₃N₂OPS
Molecular Weight:416.568
Hs Code.:

C<sub>23</sub>H<sub>33</sub>N<sub>2</sub>OPS

Synonyms:C₂₃H₃₃N₂OPS

Suppliers and Price of C₂₃H₃₃N₂OPS

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₃H₃₃N₂OPS

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₃H₃₃N₂OPS

There total 8 articles about C₂₃H₃₃N₂OPS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: bis{4-[(N,N-dimethylamino)ethyl]phenyl}(acetylthiomethyl)phosphine tris(borane)

: 952301-65-4
C₂₃H₃₃N₂OPS

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In toluene; at 40 ℃; for 4h;
DOI:10.1021/ja073204p

Reference yield:

: 15221-61-1
2-(4-bromophenyl)-N,N-dimethylethan-1-amine

: 952301-65-4
C₂₃H₃₃N₂OPS

Guidance literature:: Multi-step reaction with 6 steps

1.1: magnesium / tetrahydrofuran / 2 h / Inert atmosphere; Reflux

1.2: 0 - 23 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: water; potassium hydroxide / tetrahydrofuran; dichloromethane / 23 °C

4.1: triethylamine / dichloromethane / 0 - 23 °C

5.1: N,N-dimethyl-formamide / 23 °C / Inert atmosphere

6.1: 1,4-diaza-bicyclo[2.2.2]octane / toluene / 4 h / 40 °C / Inert atmosphere

With 1,4-diaza-bicyclo[2.2.2]octane; water; diisobutylaluminium hydride; magnesium; triethylamine; potassium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 114369-15-2
2-(4-bromophenyl)ethyl methanesulfonate

: 952301-65-4
C₂₃H₃₃N₂OPS

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetrahydrofuran / 16 h / 45 °C / Inert atmosphere

2.1: magnesium / tetrahydrofuran / 2 h / Inert atmosphere; Reflux

2.2: 0 - 23 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: water; potassium hydroxide / tetrahydrofuran; dichloromethane / 23 °C

5.1: triethylamine / dichloromethane / 0 - 23 °C

6.1: N,N-dimethyl-formamide / 23 °C / Inert atmosphere

7.1: 1,4-diaza-bicyclo[2.2.2]octane / toluene / 4 h / 40 °C / Inert atmosphere

With 1,4-diaza-bicyclo[2.2.2]octane; water; diisobutylaluminium hydride; magnesium; triethylamine; potassium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;