(1-methyl-2-diphenylphosphino-3-methylimidazolium)chlorogold(I) triflate

Base Information

Chemical Name:(1-methyl-2-diphenylphosphino-3-methylimidazolium)chlorogold(I) triflate
CAS No.:1610951-42-2
Molecular Formula:CF₃O₃S*C₁₇H₁₈AuClN₂P
Molecular Weight:662.807
Hs Code.:

Synonyms:(1-methyl-2-diphenylphosphino-3-methylimidazolium)chlorogold(I) triflate

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Chemical Property of (1-methyl-2-diphenylphosphino-3-methylimidazolium)chlorogold(I) triflate

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Technology Process of (1-methyl-2-diphenylphosphino-3-methylimidazolium)chlorogold(I) triflate

There total 3 articles about (1-methyl-2-diphenylphosphino-3-methylimidazolium)chlorogold(I) triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 39929-21-0
(tetrahydrothiophene)gold(I) chloride

: 1379677-77-6
1-methyl-2-diphenylphosphino-3-methylimidazolium triflate

: 1610951-42-2
(1-methyl-2-diphenylphosphino-3-methylimidazolium)chlorogold(I) triflate

Guidance literature:: In dichloromethane; at 20 ℃; for 0.25h;
DOI:10.1016/j.jorganchem.2014.04.005

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1610951-42-2
(1-methyl-2-diphenylphosphino-3-methylimidazolium)chlorogold(I) triflate

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium / tetrahydrofuran; hexane / 4 h / -78 - 20 °C / Inert atmosphere

2: dichloromethane / 1 h / -78 °C / Inert atmosphere

3: dichloromethane / 0.25 h / 20 °C

With n-butyllithium; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1016/j.jorganchem.2014.04.005

Reference yield:

: 150404-18-5
(1-methylimidazol-2-yl)diphenylphosphine

: 1610951-42-2
(1-methyl-2-diphenylphosphino-3-methylimidazolium)chlorogold(I) triflate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 1 h / -78 °C / Inert atmosphere

2: dichloromethane / 0.25 h / 20 °C

In dichloromethane;
DOI:10.1016/j.jorganchem.2014.04.005