4-Oxo-α-(p-tolyl)-2,5-cyclohexadien-Δ^1α-acetonitriloxim

Base Information

Chemical Name:4-Oxo-α-(p-tolyl)-2,5-cyclohexadien-Δ^1α-acetonitriloxim
CAS No.:22074-90-4
Molecular Formula:C₁₅H₁₂N₂O
Molecular Weight:236.273
Hs Code.:

4-Oxo-α-(p-tolyl)-2,5-cyclohexadien-Δ<sup>1α</sup>-acetonitriloxim

Synonyms:4-Oxo-α-(p-tolyl)-2,5-cyclohexadien-Δ^1α-acetonitriloxim

Suppliers and Price of 4-Oxo-α-(p-tolyl)-2,5-cyclohexadien-Δ^1α-acetonitriloxim

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Oxo-α-(p-tolyl)-2,5-cyclohexadien-Δ^1α-acetonitriloxim

Chemical Property:

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Technology Process of 4-Oxo-α-(p-tolyl)-2,5-cyclohexadien-Δ^1α-acetonitriloxim

There total 1 articles about 4-Oxo-α-(p-tolyl)-2,5-cyclohexadien-Δ^1α-acetonitriloxim which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2947-61-7
(4-methylphenyl)acetonitrile

: 98-95-3,26969-40-4
nitrobenzene

: 22074-90-4
4-Oxo-α-(p-tolyl)-2,5-cyclohexadien-Δ^1α-acetonitriloxim

Guidance literature:: With potassium hydroxide; In methanol;

Reference yield:

: 2947-61-7
(4-methylphenyl)acetonitrile

: 22074-90-4
(4-Hydroxyimino-cyclohexa-2,5-dienylidene)-(4-methylphenyl)-acetonitrile

: 124-63-0
methanesulfonyl chloride

: 219650-71-2
(4-Methylsulfonyloxyimino-cyclohexa-2,5-dienylidene)-(4-methylphenyl)-acetonitrile

Guidance literature:: With potassium hydroxide; acetic acid; triethylamine; In tetrahydrofuran; methanol; water; nitrobenzene;

Reference yield:

: 22074-90-4
4-Oxo-α-(p-tolyl)-2,5-cyclohexadien-Δ^1α-acetonitriloxim

: (+/-)-2-(p-Tolyl)-2-(p-aminophenyl)-ethylamin

Guidance literature:: Multi-step reaction with 2 steps

1: Zn-Hg / acetic acid

2: H₂, NH₃ / Raney-Ni / tetrahydrofuran

With ammonia; hydrogen; mercury; zinc; nickel; In tetrahydrofuran; acetic acid;
DOI:10.1021/jm00301a003