N-(4-n-tetradecyloxysalicylidene)-4'-n-octadecyloxyaniline

Base Information

• Chemical Name: N-(4-n-tetradecyloxysalicylidene)-4'-n-octadecyloxyaniline
• CAS No.: 1609246-33-4
• Molecular Formula: C₄₅H₇₅NO₃
• Molecular Weight: 678.095
• Mol file: 1609246-33-4.mol

Synonyms:N-(4-n-tetradecyloxysalicylidene)-4'-n-octadecyloxyaniline

Chemical Property of N-(4-n-tetradecyloxysalicylidene)-4'-n-octadecyloxyaniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(4-n-tetradecyloxysalicylidene)-4'-n-octadecyloxyaniline

There total 5 articles about N-(4-n-tetradecyloxysalicylidene)-4'-n-octadecyloxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-(octadecyloxy)aniline (4105-89-9) + 2-hydroxy-4-tetradecyloxybenzaldehyde (97716-58-0) → N-(4-n-tetradecyloxysalicylidene)-4'-n-octadecyloxyaniline (1609246-33-4)

Guidance literature:

With acetic acid; In ethanol; Reflux;

DOI:10.1016/j.molstruc.2014.03.006

Reference yield:

4-acetaminophenol (103-90-2,8055-08-1) → N-(4-n-tetradecyloxysalicylidene)-4'-n-octadecyloxyaniline (1609246-33-4)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate; potassium iodide / acetone / 36 h / Reflux

2: hydrogenchloride / water; ethanol / 4 h

3: acetic acid / ethanol / Reflux

With hydrogenchloride; potassium carbonate; acetic acid; potassium iodide; In ethanol; water; acetone;

DOI:10.1016/j.molstruc.2014.03.006

Reference yield:

N-(4-(octadecyloxy)phenyl)acetamide (73722-04-0) → N-(4-n-tetradecyloxysalicylidene)-4'-n-octadecyloxyaniline (1609246-33-4)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride / water; ethanol / 4 h

2: acetic acid / ethanol / Reflux

With hydrogenchloride; acetic acid; In ethanol; water;

DOI:10.1016/j.molstruc.2014.03.006

upstream raw materials:

4-(octadecyloxy)aniline

2-hydroxy-4-tetradecyloxybenzaldehyde

4-acetaminophenol

N-(4-(octadecyloxy)phenyl)acetamide

Downstream raw materials:

C₉₀H₁₄₈N₂O₇V