7β-Methyl-5-phenylsulphonyl-5,6,6aβ,7,8,9,10,10aβ-octahydroindeno<2,1-b>indol-6α-ol

Base Information

Chemical Name:7β-Methyl-5-phenylsulphonyl-5,6,6aβ,7,8,9,10,10aβ-octahydroindeno<2,1-b>indol-6α-ol
CAS No.:137531-69-2
Molecular Formula:C₂₂H₂₃NO₃S
Molecular Weight:381.496
Hs Code.:

Synonyms:7β-Methyl-5-phenylsulphonyl-5,6,6aβ,7,8,9,10,10aβ-octahydroindeno<2,1-b>indol-6α-ol

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Chemical Property of 7β-Methyl-5-phenylsulphonyl-5,6,6aβ,7,8,9,10,10aβ-octahydroindeno<2,1-b>indol-6α-ol

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Technology Process of 7β-Methyl-5-phenylsulphonyl-5,6,6aβ,7,8,9,10,10aβ-octahydroindeno<2,1-b>indol-6α-ol

There total 5 articles about 7β-Methyl-5-phenylsulphonyl-5,6,6aβ,7,8,9,10,10aβ-octahydroindeno<2,1-b>indol-6α-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 132430-79-6,137623-47-3
7β-Methyl-6-oxo-5-phenylsulphonyl-5,6,6aβ,7,8,9,10,10aβ-octahydroindeno<2,1-b>indole

: 137531-69-2
7β-Methyl-5-phenylsulphonyl-5,6,6aβ,7,8,9,10,10aβ-octahydroindeno<2,1-b>indol-6α-ol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1h;

Reference yield:

: 63883-66-9
2-methylcyclohexanone (2,4,6-triisopropylphenyl)sulphonylhydrazone

: 137531-69-2
7β-Methyl-5-phenylsulphonyl-5,6,6aβ,7,8,9,10,10aβ-octahydroindeno<2,1-b>indol-6α-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) tert-bytyllithium / 1.) THF, -70 degC to r.t., 2.) THF, -70 degC to r.t., overnight

2: 68 percent / MnO₂ / benzene / 12 h / Ambient temperature

3: AlCl₃ / benzene / 20 h / Ambient temperature

4: 90 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; aluminium trichloride; tert.-butyl lithium; In tetrahydrofuran; benzene;

Reference yield:

: 137531-66-9,137531-67-0
(6-Methylcyclohex-1-enyl)(1'-phenylsulphonylindol-2'-yl)methanol

: 137531-69-2
7β-Methyl-5-phenylsulphonyl-5,6,6aβ,7,8,9,10,10aβ-octahydroindeno<2,1-b>indol-6α-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / MnO₂ / benzene / 12 h / Ambient temperature

2: AlCl₃ / benzene / 20 h / Ambient temperature

3: 90 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; aluminium trichloride; In tetrahydrofuran; benzene;