3-(5-(1-methyl-1H-pyrazol-4-yl)-1H-benzo[d]imidazol-1-yl)-5-(1H-pyrrol-1-yl)aniline

Base Information

Chemical Name:3-(5-(1-methyl-1H-pyrazol-4-yl)-1H-benzo[d]imidazol-1-yl)-5-(1H-pyrrol-1-yl)aniline
CAS No.:1430727-93-7
Molecular Formula:C₂₁H₁₈N₆
Molecular Weight:354.414
Hs Code.:

Synonyms:3-(5-(1-methyl-1H-pyrazol-4-yl)-1H-benzo[d]imidazol-1-yl)-5-(1H-pyrrol-1-yl)aniline

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Chemical Property of 3-(5-(1-methyl-1H-pyrazol-4-yl)-1H-benzo[d]imidazol-1-yl)-5-(1H-pyrrol-1-yl)aniline

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Technology Process of 3-(5-(1-methyl-1H-pyrazol-4-yl)-1H-benzo[d]imidazol-1-yl)-5-(1H-pyrrol-1-yl)aniline

There total 9 articles about 3-(5-(1-methyl-1H-pyrazol-4-yl)-1H-benzo[d]imidazol-1-yl)-5-(1H-pyrrol-1-yl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1430724-17-6
N-(3-(5-(1-methyl-1H-pyrazol-4-yl)-1H-benzo[d]imidazol-1-yl)-5-(1H-pyrrol-1-yl)phenyl)acetamide

: 1430727-93-7
3-(5-(1-methyl-1H-pyrazol-4-yl)-1H-benzo[d]imidazol-1-yl)-5-(1H-pyrrol-1-yl)aniline

Guidance literature:: With sodium hydroxide; In ethanol; at 100 ℃; for 2h;

Reference yield:

: 618-87-1
3, 5-dinitroaniline

: 1430727-93-7
3-(5-(1-methyl-1H-pyrazol-4-yl)-1H-benzo[d]imidazol-1-yl)-5-(1H-pyrrol-1-yl)aniline

Guidance literature:: Multi-step reaction with 9 steps

1: acetic acid / 16 h / 100 °C

2: diammonium sulfide; pyridine / water; ethanol / 4 h / 80 °C

3: 0.5 h / 20 °C

4: water; calcium chloride; iron / ethanol / 2 h / 80 °C

5: potassium fluoride / N,N-dimethyl-formamide / 110 °C

6: water; calcium chloride; iron / ethanol / 2 h / 80 °C

7: 2 h / 20 - 100 °C

8: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 2 h / 100 °C / Inert atmosphere

9: sodium hydroxide / ethanol / 2 h / 100 °C

With pyridine; diammonium sulfide; potassium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; iron; sodium carbonate; acetic acid; calcium chloride; sodium hydroxide; In 1,2-dimethoxyethane; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 321329-77-5
1-(3,5-dinitro-phenyl)-1H-pyrrole

: 1430727-93-7
3-(5-(1-methyl-1H-pyrazol-4-yl)-1H-benzo[d]imidazol-1-yl)-5-(1H-pyrrol-1-yl)aniline

Guidance literature:: Multi-step reaction with 8 steps

1: diammonium sulfide; pyridine / water; ethanol / 4 h / 80 °C

2: 0.5 h / 20 °C

3: water; calcium chloride; iron / ethanol / 2 h / 80 °C

4: potassium fluoride / N,N-dimethyl-formamide / 110 °C

5: water; calcium chloride; iron / ethanol / 2 h / 80 °C

6: 2 h / 20 - 100 °C

7: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 2 h / 100 °C / Inert atmosphere

8: sodium hydroxide / ethanol / 2 h / 100 °C

With pyridine; diammonium sulfide; potassium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; iron; sodium carbonate; calcium chloride; sodium hydroxide; In 1,2-dimethoxyethane; ethanol; water; N,N-dimethyl-formamide;