2,3,4,6-tetra-O-acetyl-α-D-talopyranosyl bromide

Base Information

Chemical Name:2,3,4,6-tetra-O-acetyl-α-D-talopyranosyl bromide
CAS No.:14227-54-4
Molecular Formula:C₁₄H₁₉BrO₉
Molecular Weight:411.203
Hs Code.:

Synonyms:2,3,4,6-tetra-O-acetyl-α-D-talopyranosyl bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3,4,6-tetra-O-acetyl-α-D-talopyranosyl bromide

Chemical Property:

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Technology Process of 2,3,4,6-tetra-O-acetyl-α-D-talopyranosyl bromide

There total 36 articles about 2,3,4,6-tetra-O-acetyl-α-D-talopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 604-69-3
β-D-glucose pentaacetate

: 572-09-8,3068-32-4,4026-32-8,6919-96-6,13242-53-0,14227-54-4,14795-18-7,19186-59-5,19285-38-2,21698-13-5,29907-26-4,53369-42-9,60619-58-1,61303-35-3,67337-79-5,69127-37-3,70749-15-4,72002-90-5,75247-30-2,75880-74-9,78418-57-2,102339-89-9,102339-90-2,103530-40-1,114028-03-4,114718-45-5,138514-70-2,138514-71-3
2,3,4,6-tetra-O-acetyl-D-glucopyranosyl bromide

Guidance literature:: With hydrogen bromide; acetic acid; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1016/j.bioorg.2021.105479

Reference yield: 100.0%

: 83-87-4,604-68-2,604-69-3,2152-77-4,4026-35-1,4163-59-1,4163-60-4,4163-61-5,4163-65-9,4257-94-7,4257-96-9,16299-15-3,19186-39-1,19189-55-0,25878-60-8,25941-03-1,32445-48-0,32445-49-1,32445-53-7,32445-54-8,34685-58-0,34685-59-1,43168-42-9,43168-44-1,43169-22-8,43169-25-1,66966-07-2,70749-17-6,80184-01-6,93221-01-3,93221-02-4,99630-88-3,109215-53-4,115792-70-6,115792-73-9,139894-92-1,139973-25-4,144071-49-8,147648-81-5
D-glucose pentaacetate

: 572-09-8,3068-32-4,4026-32-8,6919-96-6,13242-53-0,14227-54-4,14795-18-7,19186-59-5,19285-38-2,21698-13-5,29907-26-4,53369-42-9,60619-58-1,61303-35-3,67337-79-5,69127-37-3,70749-15-4,72002-90-5,75247-30-2,75880-74-9,78418-57-2,102339-89-9,102339-90-2,103530-40-1,114028-03-4,114718-45-5,138514-70-2,138514-71-3
2,3,4,6-tetra-O-acetyl-D-glucopyranosyl bromide

Guidance literature:: With hydrogen bromide; In acetic acid; at 20 ℃; Sealed tube;

Reference yield: 83.0%

: 2280-44-6
D-Glucose

: 108-24-7
acetic anhydride

: 572-09-8,3068-32-4,4026-32-8,6919-96-6,13242-53-0,14227-54-4,14795-18-7,19186-59-5,19285-38-2,21698-13-5,29907-26-4,53369-42-9,60619-58-1,61303-35-3,67337-79-5,69127-37-3,70749-15-4,72002-90-5,75247-30-2,75880-74-9,78418-57-2,102339-89-9,102339-90-2,103530-40-1,114028-03-4,114718-45-5,138514-70-2,138514-71-3
2,3,4,6-tetra-O-acetyl-D-glucopyranosyl bromide

Guidance literature:: D-Glucose; acetic anhydride; With perchloric acid; at 20 ℃; for 4h;

With phosphorus; bromine; In water; at 20 ℃; for 3h;
DOI:10.1007/s10600-016-1721-5