pyrrolo[3',4':5,6][1,4]diphosphorino[2,3-c]pyrrole-2,4,4,4,6,8,8,8-octahydro-1,3,5,7-tetramethyl-2,6-bis(4-methylphenyl)-4,8-dioxide

Base Information

Chemical Name:pyrrolo[3',4':5,6][1,4]diphosphorino[2,3-c]pyrrole-2,4,4,4,6,8,8,8-octahydro-1,3,5,7-tetramethyl-2,6-bis(4-methylphenyl)-4,8-dioxide
CAS No.:308798-37-0
Molecular Formula:C₂₆H₂₈N₂O₂P₂
Molecular Weight:462.468
Hs Code.:

Synonyms:pyrrolo[3',4':5,6][1,4]diphosphorino[2,3-c]pyrrole-2,4,4,4,6,8,8,8-octahydro-1,3,5,7-tetramethyl-2,6-bis(4-methylphenyl)-4,8-dioxide

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Chemical Property of pyrrolo[3',4':5,6][1,4]diphosphorino[2,3-c]pyrrole-2,4,4,4,6,8,8,8-octahydro-1,3,5,7-tetramethyl-2,6-bis(4-methylphenyl)-4,8-dioxide

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Technology Process of pyrrolo[3',4':5,6][1,4]diphosphorino[2,3-c]pyrrole-2,4,4,4,6,8,8,8-octahydro-1,3,5,7-tetramethyl-2,6-bis(4-methylphenyl)-4,8-dioxide

There total 4 articles about pyrrolo[3',4':5,6][1,4]diphosphorino[2,3-c]pyrrole-2,4,4,4,6,8,8,8-octahydro-1,3,5,7-tetramethyl-2,6-bis(4-methylphenyl)-4,8-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 308798-35-8
pyrrolo[3',4':5,6][1,4]diphosphorino[2,3-c]pyrrole-14,8-dibromo-2,4,6,8-tetrahydro-1,3,5,7-tetramethyl-2,6-bis(4-methylphenyl)

: 308798-37-0
pyrrolo[3',4':5,6][1,4]diphosphorino[2,3-c]pyrrole-2,4,4,4,6,8,8,8-octahydro-1,3,5,7-tetramethyl-2,6-bis(4-methylphenyl)-4,8-dioxide

Guidance literature:: With water; In dichloromethane; for 24h;
DOI:10.1007/BF02269561

Reference yield:

: 5044-26-8
2,5-dimethyl-1-p-tolyl-1H-pyrrole

: 308798-37-0
pyrrolo[3',4':5,6][1,4]diphosphorino[2,3-c]pyrrole-2,4,4,4,6,8,8,8-octahydro-1,3,5,7-tetramethyl-2,6-bis(4-methylphenyl)-4,8-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1: phosphorus tribromide / pyridine

2: 74 percent / phosphorus tribromide / pyridine / 74 h

3: 53 percent / CH₂Cl₂; H₂O / 24 h

With phosphorus tribromide; In pyridine; dichloromethane; water;
DOI:10.1002/hc.1105

Reference yield:

: C₂₆H₂₈BrN₂P

: 308798-37-0
pyrrolo[3',4':5,6][1,4]diphosphorino[2,3-c]pyrrole-2,4,4,4,6,8,8,8-octahydro-1,3,5,7-tetramethyl-2,6-bis(4-methylphenyl)-4,8-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / phosphorus tribromide / pyridine / 74 h

2: 53 percent / CH₂Cl₂; H₂O / 24 h

With phosphorus tribromide; In pyridine; dichloromethane; water;
DOI:10.1002/hc.1105