3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(benzyloxy)hexaethylene glycol acetylthymidine

Base Information

Chemical Name:3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(benzyloxy)hexaethylene glycol acetylthymidine
CAS No.:1361209-04-2
Molecular Formula:C₅₅H₈₃N₃O₁₄
Molecular Weight:1010.28
Hs Code.:

Synonyms:3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(benzyloxy)hexaethylene glycol acetylthymidine

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Chemical Property of 3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(benzyloxy)hexaethylene glycol acetylthymidine

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Technology Process of 3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(benzyloxy)hexaethylene glycol acetylthymidine

There total 10 articles about 3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(benzyloxy)hexaethylene glycol acetylthymidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 185990-10-7
20-benzyloxy-3,6,9,12,15,18-hexaoxaeicosanoic acid

: 1361208-83-4
3-(4-pyridylmethyl)-3’-O-oleyl-thymidine

: 1361209-04-2
3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(benzyloxy)hexaethylene glycol acetylthymidine

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1039/c1mb05143a

Reference yield:

: 1361208-77-6
3-(4-pyridylmethyl)-5’-O-(4,4′-dimethoxytriphenylmethyl)-thymidine

: 1361209-04-2
3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(benzyloxy)hexaethylene glycol acetylthymidine

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 12 h / 20 °C

2: trichloroacetic acid / dichloromethane / 1 h / 20 °C

3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 4 h / 20 °C

With dmap; dicyclohexyl-carbodiimide; trichloroacetic acid; In dichloromethane;
DOI:10.1039/c1mb05143a

Reference yield:

: 1361208-80-1
3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(4,4′-dimethoxytriphenylmethyl)-thymidine

: 1361209-04-2
3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(benzyloxy)hexaethylene glycol acetylthymidine

Guidance literature:: Multi-step reaction with 2 steps

1: trichloroacetic acid / dichloromethane / 1 h / 20 °C

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 4 h / 20 °C

With dmap; dicyclohexyl-carbodiimide; trichloroacetic acid; In dichloromethane;
DOI:10.1039/c1mb05143a