3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(4,4′-dimethoxytriphenylmethyl)-thymidine

Base Information

Chemical Name:3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(4,4′-dimethoxytriphenylmethyl)-thymidine
CAS No.:1361208-80-1
Molecular Formula:C₅₅H₆₉N₃O₈
Molecular Weight:900.168
Hs Code.:

Synonyms:3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(4,4′-dimethoxytriphenylmethyl)-thymidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(4,4′-dimethoxytriphenylmethyl)-thymidine

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Technology Process of 3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(4,4′-dimethoxytriphenylmethyl)-thymidine

There total 4 articles about 3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(4,4′-dimethoxytriphenylmethyl)-thymidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 112-80-1,2027-47-6
cis-Octadecenoic acid

: 1361208-77-6
3-(4-pyridylmethyl)-5’-O-(4,4′-dimethoxytriphenylmethyl)-thymidine

: 1361208-80-1
3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(4,4′-dimethoxytriphenylmethyl)-thymidine

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1039/c8tb01563e

Reference yield:

: 40615-39-2
5'-O-(4-4'-dimethoxytrityl)thymidine

: 1361208-80-1
3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(4,4′-dimethoxytriphenylmethyl)-thymidine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 60 °C

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 12 h / 20 °C

With dmap; potassium carbonate; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c1mb05143a

Reference yield:

: 54751-01-8
4-(bromomethyl)pyridine

: 1361208-80-1
3-(4-pyridylmethyl)-3’-O-oleyl-5’-O-(4,4′-dimethoxytriphenylmethyl)-thymidine

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 20 h / 60 °C

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 15 h / 20 °C

With dmap; caesium carbonate; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c8tb01563e