(4E,8Z)-8-Benzyloxy-4-hydroxymethyl-8-methyl-4,8-decadienal ethylene acetal

Base Information

Chemical Name:(4E,8Z)-8-Benzyloxy-4-hydroxymethyl-8-methyl-4,8-decadienal ethylene acetal
CAS No.:125556-29-8
Molecular Formula:C₂₁H₃₀O₄
Molecular Weight:346.467
Hs Code.:

Synonyms:(4E,8Z)-8-Benzyloxy-4-hydroxymethyl-8-methyl-4,8-decadienal ethylene acetal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4E,8Z)-8-Benzyloxy-4-hydroxymethyl-8-methyl-4,8-decadienal ethylene acetal

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Technology Process of (4E,8Z)-8-Benzyloxy-4-hydroxymethyl-8-methyl-4,8-decadienal ethylene acetal

There total 10 articles about (4E,8Z)-8-Benzyloxy-4-hydroxymethyl-8-methyl-4,8-decadienal ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 116187-20-3
10-benzyloxy-8-methyl-4-formyldeca-4E,8Z-dien-1-al ethyleneacetal

: 125556-29-8
(4E,8Z)-8-Benzyloxy-4-hydroxymethyl-8-methyl-4,8-decadienal ethylene acetal

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 20 ℃; for 1.5h;
DOI:10.1007/BF00963008

Reference yield:

: 18742-02-4
2-bromo-2-(2-ethyl)dioxolane

: 125556-29-8
(4E,8Z)-8-Benzyloxy-4-hydroxymethyl-8-methyl-4,8-decadienal ethylene acetal

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) LDA, HMPT / 1.) hexane, THF, 0 deg C, 20 min, 2.) -50 deg C, 4 h

2: 1.) LDA / 1.) hexane, THF, -5 deg C, 40 min, 2.) -40 deg C, 4 h

4: 90 percent / NaBH₄ / ethanol / 1.5 h / 25 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; lithium diisopropyl amide; In ethanol;
DOI:10.1055/s-1989-27327

Reference yield:

: 116187-17-8
5,5-Ethylenedioxypentanal tert-butylimine

: 125556-29-8
(4E,8Z)-8-Benzyloxy-4-hydroxymethyl-8-methyl-4,8-decadienal ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA / 1.) hexane, THF, -5 deg C, 40 min, 2.) -40 deg C, 4 h

3: 90 percent / NaBH₄ / ethanol / 1.5 h / 25 °C

With sodium tetrahydroborate; lithium diisopropyl amide; In ethanol;
DOI:10.1055/s-1989-27327