N-benzyl-N-vinylisonicotinamide

Base Information

Chemical Name:N-benzyl-N-vinylisonicotinamide
CAS No.:1429043-76-4
Molecular Formula:C₁₅H₁₄N₂O
Molecular Weight:238.289
Hs Code.:

Synonyms:N-benzyl-N-vinylisonicotinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl-N-vinylisonicotinamide

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Technology Process of N-benzyl-N-vinylisonicotinamide

There total 3 articles about N-benzyl-N-vinylisonicotinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 1271436-27-1
N-benzyl-N-(2-chloroethyl)isonicotinamide

: 1429043-76-4
N-benzyl-N-vinylisonicotinamide

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; at 20 ℃; for 60h; Inert atmosphere;
DOI:10.1021/ol400571j

Reference yield:

: 55-22-1
pyridine-4-carboxylic acid

: 1429043-76-4
N-benzyl-N-vinylisonicotinamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / 2 h / Inert atmosphere

2.1: pyridine / dichloromethane / 0.03 h / 0 °C / Inert atmosphere; Molecular sieve

2.2: 0 - 20 °C / Inert atmosphere

3.1: potassium tert-butylate / tert-butyl alcohol / 60 h / 20 °C / Inert atmosphere

With pyridine; thionyl chloride; potassium tert-butylate; In dichloromethane; tert-butyl alcohol;
DOI:10.1021/ol400571j

Reference yield:

: 14254-57-0
4-(chlorocarbonyl)pyridine

: 1429043-76-4
N-benzyl-N-vinylisonicotinamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / dichloromethane / 0.03 h / 0 °C / Inert atmosphere; Molecular sieve

1.2: 0 - 20 °C / Inert atmosphere

2.1: potassium tert-butylate / tert-butyl alcohol / 60 h / 20 °C / Inert atmosphere

With pyridine; potassium tert-butylate; In dichloromethane; tert-butyl alcohol;
DOI:10.1021/ol400571j