C₃₀H₄₃BrFNO₅Si

Base Information

Chemical Name:C₃₀H₄₃BrFNO₅Si
CAS No.:1311411-82-1
Molecular Formula:C₃₀H₄₃BrFNO₅Si
Molecular Weight:624.663
Hs Code.:

C<sub>30</sub>H<sub>43</sub>BrFNO<sub>5</sub>Si

Synonyms:C₃₀H₄₃BrFNO₅Si

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Chemical Property of C₃₀H₄₃BrFNO₅Si

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Technology Process of C₃₀H₄₃BrFNO₅Si

There total 15 articles about C₃₀H₄₃BrFNO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1311411-80-9
C₂₄H₂₉BrFNO₅

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1311411-82-1
C₃₀H₄₃BrFNO₅Si

Guidance literature:: C₂₄H₂₉BrFNO₅; tert-butyldimethylsilyl chloride; With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃;

With methanol; In N,N-dimethyl-formamide;

Reference yield:

: 1311410-93-1
C₁₈H₂₄BrNO₃

: 1311411-82-1
C₃₀H₄₃BrFNO₅Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium periodate; ruthenium(III) chloride trihydrate / water; acetone / 1 h / 20 °C

2.1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 0.33 h / 20 °C

2.2: 7.33 h / 20 °C

3.1: sodium tri-sec-butylborohydride / tetrahydrofuran / 1.5 h / -65 - -35 °C / Inert atmosphere

3.2: 0 - 10 °C

4.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

4.2: 1.5 h / -78 °C

5.1: sodium hydroxide / water; methanol / 3 h / 20 °C

5.2: pH 2 - 3

6.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

With 1H-imidazole; sodium periodate; ruthenium(III) chloride trihydrate; sodium tri-sec-butylborohydride; potassium hydrogencarbonate; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1311410-99-7
C₁₈H₂₄BrNO₅

: 1311411-82-1
C₃₀H₄₃BrFNO₅Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tri-sec-butylborohydride / tetrahydrofuran / 1.5 h / -65 - -35 °C / Inert atmosphere

1.2: 0 - 10 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 1.5 h / -78 °C

3.1: sodium hydroxide / water; methanol / 3 h / 20 °C

3.2: pH 2 - 3

4.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

With 1H-imidazole; sodium tri-sec-butylborohydride; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;