2-[N-tert-butyl-N-(2-methyl-1-phenyl-propyl)-aminooxy]-malonic acid dimethyl ester

Base Information

• Chemical Name: 2-[N-tert-butyl-N-(2-methyl-1-phenyl-propyl)-aminooxy]-malonic acid dimethyl ester
• CAS No.: 853886-65-4
• Molecular Formula: C₁₉H₂₉NO₅
• Molecular Weight: 351.443

Synonyms:2-[N-tert-butyl-N-(2-methyl-1-phenyl-propyl)-aminooxy]-malonic acid dimethyl ester

Chemical Property of 2-[N-tert-butyl-N-(2-methyl-1-phenyl-propyl)-aminooxy]-malonic acid dimethyl ester

Chemical Property:

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Technology Process of 2-[N-tert-butyl-N-(2-methyl-1-phenyl-propyl)-aminooxy]-malonic acid dimethyl ester

There total 1 articles about 2-[N-tert-butyl-N-(2-methyl-1-phenyl-propyl)-aminooxy]-malonic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

N-(tert-butyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl (61015-94-9) + malonic acid dimethyl ester (108-59-8) → 2-[N-tert-butyl-N-(2-methyl-1-phenyl-propyl)-aminooxy]-malonic acid dimethyl ester (853886-65-4)

Guidance literature:

malonic acid dimethyl ester; With lithium diisopropyl amide; In 1,2-dimethoxyethane; hexane; at -60 ℃; for 0.5h;

N-(tert-butyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl; With copper dichloride; In 1,2-dimethoxyethane; hexane; at 0 - 20 ℃; for 6.5h;

DOI:10.1002/chem.200400936

Reference yield: 77.0%

2-[N-tert-butyl-N-(2-methyl-1-phenyl-propyl)-aminooxy]-malonic acid dimethyl ester (853886-65-4) + oct-1-ene (111-66-0,25068-25-1) → 2-{2-[N-tert-butyl-N-(2-methyl-1-phenyl-propyl)-aminooxy]-octyl}-malonic acid dimethyl ester

Guidance literature:

In 1,2-dichloro-ethane; at 125 ℃; for 7h;

DOI:10.1002/chem.200400936

Reference yield:

2-[N-tert-butyl-N-(2-methyl-1-phenyl-propyl)-aminooxy]-malonic acid dimethyl ester (853886-65-4) → N-(tert-butyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl (61015-94-9) + C5H7O4

Guidance literature:

at 130 ℃; Activation energy;

DOI:10.1002/chem.200400936

upstream raw materials:

N-(tert-butyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl

malonic acid dimethyl ester

Downstream raw materials:

N-(tert-butyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl

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