2-(3-nitrobenzylcarbamoyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:2-(3-nitrobenzylcarbamoyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside
CAS No.:1312289-86-3
Molecular Formula:C₂₃H₂₆N₂O₈S
Molecular Weight:490.534
Hs Code.:

Synonyms:2-(3-nitrobenzylcarbamoyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside

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Chemical Property of 2-(3-nitrobenzylcarbamoyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside

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Technology Process of 2-(3-nitrobenzylcarbamoyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside

There total 7 articles about 2-(3-nitrobenzylcarbamoyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1312290-00-8
2-(3-nitrobenzylcarbamoyl)phenyl 2,4,6-tri-O-acetyl-3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside

: 1312289-86-3
2-(3-nitrobenzylcarbamoyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside

Guidance literature:: With methanol; sodium methylate; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2011.03.022

Reference yield:

: 1312289-97-6
2-carboxyphenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside

: 1312289-86-3
2-(3-nitrobenzylcarbamoyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; dmap / 48 h / 20 °C / Inert atmosphere

2: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 2.5 h / 20 °C / Inert atmosphere

3: methanol; sodium methylate / 20 °C / Inert atmosphere

With pyridine; methanol; dmap; sodium methylate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.03.022

Reference yield:

: 1312289-96-5
2-(methoxycarbonyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside

: 1312289-86-3
2-(3-nitrobenzylcarbamoyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: water; sodium hydroxide / methanol / 0.67 h / 20 °C / Inert atmosphere

1.2: acid resin treatment

2.1: pyridine; dmap / 48 h / 20 °C / Inert atmosphere

3.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 2.5 h / 20 °C / Inert atmosphere

4.1: methanol; sodium methylate / 20 °C / Inert atmosphere

With pyridine; methanol; dmap; water; sodium methylate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.03.022