2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyloxy)ethoxy)ethoxy)ethanol

Base Information

• Chemical Name: 2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyloxy)ethoxy)ethoxy)ethanol
• CAS No.: 1202396-89-1
• Molecular Formula: C₃₇H₆₈O₁₆
• Molecular Weight: 768.937

Synonyms:2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyloxy)ethoxy)ethoxy)ethanol

Chemical Property of 2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyloxy)ethoxy)ethoxy)ethanol

Chemical Property:

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Technology Process of 2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyloxy)ethoxy)ethoxy)ethanol

There total 8 articles about 2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyloxy)ethoxy)ethoxy)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-(2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyloxy)ethoxy)ethoxy)ethoxy)tetrahydro-2H-pyran → 2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyloxy)ethoxy)ethoxy)ethanol (1202396-89-1)

Guidance literature:

With toluene-4-sulfonic acid; In methanol; at 20 ℃; for 2h;

DOI:10.1016/j.ejmech.2013.09.019

Reference yield:

2-(2-(2-((tetrahydro-2H-pyran-2-yl)oxy)ethoxy)ethoxy)ethyl 4-methylbenzenesulfonate (69502-33-6) → 2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyloxy)ethoxy)ethoxy)ethanol (1202396-89-1)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium iodide; sodium hydride; 15-crown-5 / tetrahydrofuran / 24 h / 20 °C

2: toluene-4-sulfonic acid / methanol / 2 h / 20 °C

With 15-crown-5; sodium hydride; toluene-4-sulfonic acid; potassium iodide; In tetrahydrofuran; methanol;

DOI:10.1016/j.ejmech.2013.09.019

Reference yield:

methyl 3,4,5-Tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzoate (1096159-34-0) → 2-(2-(2-(3,4,5-tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzyloxy)ethoxy)ethoxy)ethanol (1202396-89-1)

Guidance literature:

Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 3.5 h / -5 - 25 °C

2: potassium iodide; sodium hydride; 15-crown-5 / tetrahydrofuran / 24 h / 20 °C

3: toluene-4-sulfonic acid / methanol / 2 h / 20 °C

With lithium aluminium tetrahydride; 15-crown-5; sodium hydride; toluene-4-sulfonic acid; potassium iodide; In tetrahydrofuran; methanol;

DOI:10.1016/j.ejmech.2013.09.019

upstream raw materials:

2-(2-(2-ethoxyethoxy)ethoxy)ethyl 4-methylbenzenesulfonate

methyl 3,4,5-Tris(2-(2-(2-ethoxyethoxy)ethoxy)ethoxy)benzoate

1-(hydroxymethyl)-3,4,5-tri{2-[2-(2-ethoxyethoxy)ethoxy]ethoxy}benzene

8-tosyloxy-3,6-dioxaoctanol

Downstream raw materials:

2-{2-[2-(3,4,5-tris{2-[2-(2-ethoxyethoxy)ethoxy]ethoxy}benzyloxy)ethoxy]ethoxy}ethyl methacrylate

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