cis-pentamethylbenzyl 4-<(4-nitrobenzenesulfonyl)oxy>cyclohexanecarboxylate

Base Information

Chemical Name:cis-pentamethylbenzyl 4-<(4-nitrobenzenesulfonyl)oxy>cyclohexanecarboxylate
CAS No.:223699-71-6
Molecular Formula:C₂₅H₃₁NO₇S
Molecular Weight:489.59
Hs Code.:

Synonyms:cis-pentamethylbenzyl 4-<(4-nitrobenzenesulfonyl)oxy>cyclohexanecarboxylate

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Chemical Property of cis-pentamethylbenzyl 4-<(4-nitrobenzenesulfonyl)oxy>cyclohexanecarboxylate

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Technology Process of cis-pentamethylbenzyl 4-<(4-nitrobenzenesulfonyl)oxy>cyclohexanecarboxylate

There total 4 articles about cis-pentamethylbenzyl 4-<(4-nitrobenzenesulfonyl)oxy>cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.1%

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 223699-80-7
cis-pentamethylbenzyl 4-hydroxycyclohexanecarboxylate

: 223699-71-6
cis-pentamethylbenzyl 4-<(4-nitrobenzenesulfonyl)oxy>cyclohexanecarboxylate

Guidance literature:: With triethylamine; In dichloromethane; Ambient temperature;
DOI:10.1021/jm980456f

Reference yield: 42.0%

: 4-hydroxy-cyclohexanecarboxylic acid pentamethylphenylmethyl ester

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 4-(4-nitro-benzenesulfonyloxy)-cyclohexanecarboxylic acid pentamethylphenylmethyl ester

: 223699-71-6
cis-pentamethylbenzyl 4-<(4-nitrobenzenesulfonyl)oxy>cyclohexanecarboxylate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmc.2006.01.064

Reference yield:

: 3618-04-0,75877-66-6,17159-80-7
4-hydroxycyclohexyl carboxylic acid ethyl ester

: 223699-71-6
cis-pentamethylbenzyl 4-<(4-nitrobenzenesulfonyl)oxy>cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 14.8 percent / Et₃N / dimethylformamide / Ambient temperature

2: 50.1 percent / Et₃N / CH₂Cl₂ / Ambient temperature

With triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm980456f