(R)-1-cyclohexyl-1-dimethylphenylsilylmethanol

Base Information

Chemical Name:(R)-1-cyclohexyl-1-dimethylphenylsilylmethanol
CAS No.:1020418-09-0
Molecular Formula:C₁₅H₂₄OSi
Molecular Weight:248.44
Hs Code.:

Synonyms:(R)-1-cyclohexyl-1-dimethylphenylsilylmethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-1-cyclohexyl-1-dimethylphenylsilylmethanol

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Technology Process of (R)-1-cyclohexyl-1-dimethylphenylsilylmethanol

There total 4 articles about (R)-1-cyclohexyl-1-dimethylphenylsilylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 150614-90-7
(dimethyl(phenyl)silyl)(cyclohexyl)methanone

: 1020418-09-0
(R)-1-cyclohexyl-1-dimethylphenylsilylmethanol

Guidance literature:: With TolBINAP/PICA-ruthenium(II); potassium tert-butylate; hydrogen; In ethanol; at 20 - 26 ℃; for 1.5h; under 7600.51 Torr; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/anie.200704696

Reference yield: 67.0%

: 185990-03-8
dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane

: 2043-61-0
cyclohexanecarbaldehyde

: 1020418-09-0
(R)-1-cyclohexyl-1-dimethylphenylsilylmethanol

Guidance literature:: With methanol; [Cu(MeCN)₂(S)-5,5'-bis[di(3,5-di-t-butyl-4-ethoxyphenyl)phosphino]-4,4'-bi-1,3-benzodioxole.F(HF)₂]; In tetrahydrofuran; at 20 ℃; enantioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201209020

Reference yield:

: 1512864-40-2
(cyclohexyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)dimethyl(phenyl)silane

: 1020418-09-0
(R)-1-cyclohexyl-1-dimethylphenylsilylmethanol

: C₁₅H₂₄OSi

Guidance literature:: With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; for 13h; Inert atmosphere;
DOI:10.1039/c5ob00159e