(cyclohexyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)dimethyl(phenyl)silane

Base Information

Chemical Name:(cyclohexyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)dimethyl(phenyl)silane
CAS No.:1512864-40-2
Molecular Formula:C₂₁H₃₅BO₂Si
Molecular Weight:358.404
Hs Code.:

Synonyms:(cyclohexyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)dimethyl(phenyl)silane

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Chemical Property of (cyclohexyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)dimethyl(phenyl)silane

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Technology Process of (cyclohexyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)dimethyl(phenyl)silane

There total 3 articles about (cyclohexyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)dimethyl(phenyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 910659-14-2
2-(cyclohexyl((4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)oxy)methyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 185990-03-8
dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane

: 1512864-40-2
(cyclohexyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)dimethyl(phenyl)silane

Guidance literature:: With sodium t-butanolate; In toluene; at 100 ℃; for 6h; Temperature; Mechanism; Inert atmosphere; Glovebox; Sealed tube; Schlenk technique;
DOI:10.1021/jacs.7b02518

Reference yield: 54.0%

: 34266-29-0
N′-(cyclohexylmethylene)-4-methylbenzenesulfonohydrazide

: 185990-03-8
dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane

: 1512864-40-2
(cyclohexyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)dimethyl(phenyl)silane

Guidance literature:: N′-(cyclohexylmethylene)-4-methylbenzenesulfonohydrazide; With benzyltrimethylammonium chloride; sodium hydride; In 1,4-dioxane; mineral oil; at 20 ℃; for 1h; Inert atmosphere; Schlenk technique;

dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane; In 1,4-dioxane; mineral oil; at 110 ℃; for 12h; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1021/ol403338s

Reference yield:

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1512864-40-2
(cyclohexyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)dimethyl(phenyl)silane

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol / 20 °C / Inert atmosphere

2.1: sodium hydride; benzyltrimethylammonium chloride / mineral oil; 1,4-dioxane / 1 h / 20 °C / Inert atmosphere; Schlenk technique

2.2: 12 h / 110 °C / Inert atmosphere; Schlenk technique; Sealed tube

With benzyltrimethylammonium chloride; sodium hydride; In 1,4-dioxane; methanol; mineral oil;
DOI:10.1021/ol403338s