4-(1-(4-butylphenyl)-1H-phenanthro[9,10-d]imidazol-2-yl)phenylboronic acid

Base Information

• Chemical Name: 4-(1-(4-butylphenyl)-1H-phenanthro[9,10-d]imidazol-2-yl)phenylboronic acid
• CAS No.: 1384124-32-6
• Molecular Formula: C₃₁H₂₇BN₂O₂
• Molecular Weight: 470.379

Synonyms:4-(1-(4-butylphenyl)-1H-phenanthro[9,10-d]imidazol-2-yl)phenylboronic acid

Chemical Property of 4-(1-(4-butylphenyl)-1H-phenanthro[9,10-d]imidazol-2-yl)phenylboronic acid

Chemical Property:

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Technology Process of 4-(1-(4-butylphenyl)-1H-phenanthro[9,10-d]imidazol-2-yl)phenylboronic acid

There total 4 articles about 4-(1-(4-butylphenyl)-1H-phenanthro[9,10-d]imidazol-2-yl)phenylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

2-(4-bromophenyl)-1-(4-butylphenyl)-1H-phenanthro[9,10-d]imidazole (1384124-25-7) → 4-(1-(4-butylphenyl)-1H-phenanthro[9,10-d]imidazol-2-yl)phenylboronic acid (1384124-32-6)

Guidance literature:

2-(4-bromophenyl)-1-(4-butylphenyl)-1H-phenanthro[9,10-d]imidazole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

With Trimethyl borate; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;

With hydrogenchloride; water; In tetrahydrofuran; hexane; for 3h;

DOI:10.1016/j.tet.2012.04.074

Reference yield:

4-bromo-benzaldehyde (1122-91-4) → 4-(1-(4-butylphenyl)-1H-phenanthro[9,10-d]imidazol-2-yl)phenylboronic acid (1384124-32-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: ammonium acetate; acetic acid / 3 h / Reflux

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

2.3: 3 h

With n-butyllithium; ammonium acetate; acetic acid; In tetrahydrofuran; hexane;

DOI:10.1016/j.tet.2012.04.074

Reference yield:

4-Butylaniline (104-13-2) → 4-(1-(4-butylphenyl)-1H-phenanthro[9,10-d]imidazol-2-yl)phenylboronic acid (1384124-32-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: ammonium acetate; acetic acid / 3 h / Reflux

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

2.3: 3 h

With n-butyllithium; ammonium acetate; acetic acid; In tetrahydrofuran; hexane;

DOI:10.1016/j.tet.2012.04.074

upstream raw materials:

2-(4-bromophenyl)-1-(4-butylphenyl)-1H-phenanthro[9,10-d]imidazole

4-Butylaniline

4-bromo-benzaldehyde

9,10-phenanthrenequinone

Downstream raw materials:

(E)-3-(5'-(4'-(1-(4-butylphenyl)-1H-phenanthro[9,10-d]imidazol-2-yl)biphenyl-4-yl)-2,2'-bithiophen-5-yl)-2-cyanoacrylic acid

5'-(4'-(1-(4-butylphenyl)-1H-phenanthro[9,10-d]imidazol-2-yl)biphenyl-4-yl)-2,2'-bithiophene-5-carbaldehyde

5'-(4-(1-(4-butylphenyl)-1H-phenanthro[9,10-d]imidazol-2-yl)phenyl)-2,2'-bithiophene-5-carbaldehyde

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