Benzyl-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid

Base Information

Chemical Name:Benzyl-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid
CAS No.:113921-70-3
Molecular Formula:C₄₆H₅₀O₁₃
Molecular Weight:810.895
Hs Code.:

Benzyl-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid

Synonyms:Benzyl-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid

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Chemical Property of Benzyl-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid

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Technology Process of Benzyl-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid

There total 9 articles about Benzyl-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 113879-98-4
Benzyl-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosid

: 113921-70-3
Benzyl-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid

Guidance literature:: With tri-n-butyl-tin hydride;

Reference yield:

: 85726-77-8
4-O-Benzoyl-2-brom-2,6-didesoxy-3-O-formyl-α-D-clucopyranosylbromid

: 113921-70-3
Benzyl-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: molecular sieves 4A, silver trifluoromethanesulfonate / nitromethane; toluene / 48 h / -78 °C

2: 80 percent / HCl / CH₂Cl₂; methanol / 6 h / Ambient temperature

3: 92 percent / tributyltin hydride, α,α-azobisisobutyronitrile / toluene / 2 h / 70 °C

With hydrogenchloride; 4 A molecular sieve; azobisisobutyronitrile; tri-n-butyl-tin hydride; silver trifluoromethanesulfonate; In methanol; nitromethane; dichloromethane; toluene;
DOI:10.1016/0008-6215(87)80139-8

Reference yield:

: 86448-03-5
C₃₄H₃₄Br₂O₁₀

: 113921-70-3
Benzyl-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / HCl / methanol / 15 h / Ambient temperature

2: molecular sieves 4A, silver trifluoromethanesulfonate / nitromethane; toluene / 48 h / -78 °C

3: 80 percent / HCl / CH₂Cl₂; methanol / 6 h / Ambient temperature

4: 92 percent / tributyltin hydride, α,α-azobisisobutyronitrile / toluene / 2 h / 70 °C

With hydrogenchloride; 4 A molecular sieve; azobisisobutyronitrile; tri-n-butyl-tin hydride; silver trifluoromethanesulfonate; In methanol; nitromethane; dichloromethane; toluene;
DOI:10.1016/0008-6215(87)80139-8