3-diethylgerma 1,2-diphenyl 1,2-diphospholane

Base Information

Chemical Name:3-diethylgerma 1,2-diphenyl 1,2-diphospholane
CAS No.:81744-45-8
Molecular Formula:C₁₈H₂₄GeP₂
Molecular Weight:374.926
Hs Code.:

Synonyms:3-diethylgerma 1,2-diphenyl 1,2-diphospholane

Suppliers and Price of 3-diethylgerma 1,2-diphenyl 1,2-diphospholane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-diethylgerma 1,2-diphenyl 1,2-diphospholane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3-diethylgerma 1,2-diphenyl 1,2-diphospholane

There total 2 articles about 3-diethylgerma 1,2-diphenyl 1,2-diphospholane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82322-80-3
1-(phenylphosphino)-2-(diethylbromogermyl)ethane

: 82312-25-2
(C₂H₅)2GeP(C₆H₅)

: 81744-49-2
2-diethylgerma 1-phenyl phosphetane

: 81744-45-8
3-diethylgerma 1,2-diphenyl 1,2-diphospholane

: 81744-51-6
((CH₃CH₂)2GePC₆H₅)2CH₂CH₂

: 82312-29-6
Ge(C₂H₅)2C₂H₄P(C₆H₅)P(Ge(C₂H₅)2C₆H₅)

Guidance literature:: With diethylamine; In benzene; Ge compd. soln. stirred at -30°C, 2-fold excess of diethylamine dded; centrifuged, evapd. (vac.), washed with C6H6, then with pentane, distd., not isolated, detected by NMR;

Reference yield:

: 81744-49-2
2-diethylgerma 1-phenyl phosphetane

: 81744-45-8
3-diethylgerma 1,2-diphenyl 1,2-diphospholane

: 82312-25-2
2,2-diethyl-1-phenyl-germaphosphene

Guidance literature:: In not given; byproducts: CH2CH2, Ge(CH3)2; decompn. at 120°C;

Reference yield: 73.0%

: 81744-45-8
3-diethylgerma 1,2-diphenyl 1,2-diphospholane

: 82312-29-6
Ge(C₂H₅)2C₂H₄P(C₆H₅)P(Ge(C₂H₅)2C₆H₅)

: 79301-90-9
phenyldiethylgermane

: 82312-33-2
2-(diethylgermyl)-1-(phenylphosphino)ethane

: 7803-51-2
phosphan

: 638-21-1
phenylphosphane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; LiAlH4 (2-fold excess) added in portions to educts mixt. in Et2O, refluxed for 6 h; hydrolyzed, extd. (Et2O), dried (Na2SO4), distd.; elem. anal.;