C₅₈H₈₇NO₁₃Si₂

Base Information

Chemical Name:C₅₈H₈₇NO₁₃Si₂
CAS No.:1402588-85-5
Molecular Formula:C₅₈H₈₇NO₁₃Si₂
Molecular Weight:1062.5
Hs Code.:

C<sub>58</sub>H<sub>87</sub>NO<sub>13</sub>Si<sub>2</sub>

Synonyms:C₅₈H₈₇NO₁₃Si₂

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Chemical Property of C₅₈H₈₇NO₁₃Si₂

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Technology Process of C₅₈H₈₇NO₁₃Si₂

There total 27 articles about C₅₈H₈₇NO₁₃Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1402588-84-4
C₅₁H₈₃NO₁₂Si₂

: 98-88-4
benzoyl chloride

: 1402588-85-5
C₅₈H₈₇NO₁₃Si₂

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In toluene; at 0 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ja3057612

Reference yield:

: 1402588-67-3
C₁₁H₁₄O₄

: 1402588-85-5
C₅₈H₈₇NO₁₃Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetrahydrofuran; diethyl ether / 0.5 h / 0 °C / Inert atmosphere

1.2: 0.5 h / 0 °C

1.3: 0 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / Inert atmosphere

3.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 1 h / 20 °C / Inert atmosphere

4.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / tert-butyl alcohol; water / 1.5 h / 20 °C / Inert atmosphere

5.1: dichloromethane; N,N-dimethyl-formamide / 2 h / 0 °C / Inert atmosphere

6.1: N-ethyl-N,N-diisopropylamine / toluene / 1.33 h / 40 °C

6.2: 6 h / 20 °C / Inert atmosphere

7.1: N-ethyl-N,N-diisopropylamine / toluene / 4 h / 0 °C / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1021/ja3057612

Reference yield:

: 152386-84-0
(2R,3R)-2-O-(4-methoxybenzyl)-1,2,3,4-butanetetrol

: 1402588-85-5
C₅₈H₈₇NO₁₃Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium periodate / 2 h / 0 °C / Inert atmosphere

2.1: tetrahydrofuran; diethyl ether / 0.5 h / 0 °C / Inert atmosphere

2.2: 0.5 h / 0 °C

2.3: 0 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / Inert atmosphere

4.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 1 h / 20 °C / Inert atmosphere

5.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / tert-butyl alcohol; water / 1.5 h / 20 °C / Inert atmosphere

6.1: dichloromethane; N,N-dimethyl-formamide / 2 h / 0 °C / Inert atmosphere

7.1: N-ethyl-N,N-diisopropylamine / toluene / 1.33 h / 40 °C

7.2: 6 h / 20 °C / Inert atmosphere

8.1: N-ethyl-N,N-diisopropylamine / toluene / 4 h / 0 °C / Inert atmosphere

With sodium chlorite; sodium periodate; sodium dihydrogenphosphate; 2-methyl-but-2-ene; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1021/ja3057612