(2S)-3-[4-cyano-3-(trifluoromethyl)anilino]-2-hydroxy-2-methyl-3-oxopropyl Methanesulfonate

Base Information

Chemical Name:(2S)-3-[4-cyano-3-(trifluoromethyl)anilino]-2-hydroxy-2-methyl-3-oxopropyl Methanesulfonate
CAS No.:316373-96-3
Molecular Formula:C₁₃H₁₃F₃N₂O₅S
Molecular Weight:366.318
Hs Code.:

Synonyms:(2S)-3-[4-cyano-3-(trifluoromethyl)anilino]-2-hydroxy-2-methyl-3-oxopropyl Methanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-3-[4-cyano-3-(trifluoromethyl)anilino]-2-hydroxy-2-methyl-3-oxopropyl Methanesulfonate

Chemical Property:

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Technology Process of (2S)-3-[4-cyano-3-(trifluoromethyl)anilino]-2-hydroxy-2-methyl-3-oxopropyl Methanesulfonate

There total 6 articles about (2S)-3-[4-cyano-3-(trifluoromethyl)anilino]-2-hydroxy-2-methyl-3-oxopropyl Methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90357-53-2
N-[4-cyano-3-(trifluoromethyl)phenyl]-2-methylacrylamide

: 316373-96-3
(2S)-3-[4-cyano-3-(trifluoromethyl)anilino]-2-hydroxy-2-methyl-3-oxopropyl Methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: water; tert-butyl alcohol / 168 h / 0 - 4 °C

2: triethylamine / dichloromethane / 0.58 h / 0 - 20 °C

With triethylamine; In dichloromethane; water; tert-butyl alcohol;

Reference yield:

: 316373-93-0
(2S)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2,3-dihydroxy-2-methylpropanamide

: 124-63-0
methanesulfonyl chloride

: 316373-96-3
(2S)-3-[4-cyano-3-(trifluoromethyl)anilino]-2-hydroxy-2-methyl-3-oxopropyl Methanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 0.583333h;

Reference yield:

: 654-70-6
4-amino-2-trifluoromethylbenzonitrile

: 316373-96-3
(2S)-3-[4-cyano-3-(trifluoromethyl)anilino]-2-hydroxy-2-methyl-3-oxopropyl Methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl acetamide / 3 h / 5 - 20 °C

2: water; tert-butyl alcohol / 168 h / 0 - 4 °C

3: triethylamine / dichloromethane / 0.58 h / 0 - 20 °C

With triethylamine; In dichloromethane; N,N-dimethyl acetamide; water; tert-butyl alcohol;