p-Cumaldehyd-phenylsulfonylhydrazon

Base Information

• Chemical Name: p-Cumaldehyd-phenylsulfonylhydrazon
• CAS No.: 50626-30-7
• Molecular Formula: C₁₆H₁₈N₂O₂S
• Molecular Weight: 302.397
• Mol file: 50626-30-7.mol

Synonyms:p-Cumaldehyd-phenylsulfonylhydrazon

Chemical Property of p-Cumaldehyd-phenylsulfonylhydrazon

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of p-Cumaldehyd-phenylsulfonylhydrazon

There total 2 articles about p-Cumaldehyd-phenylsulfonylhydrazon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-isopropylbenzaldehyde) (122-03-2) + benzenesufonyl hydrazide (80-17-1) → p-Cumaldehyd-phenylsulfonylhydrazon (50626-30-7)

Guidance literature:

In ethanol; at 20 ℃; for 3h; Inert atmosphere;

DOI:10.1016/j.bmc.2015.03.006

Reference yield:

→ p-Cumaldehyd-phenylsulfonylhydrazon (50626-30-7)

Guidance literature:

p-Cumaldehyd, Phenylsulfonylhydrazin;

DOI:10.1246/bcsj.49.1920

Reference yield:

(S)-methyl 3-(4-aminophenyl)-2-(((benzyloxy)carbonyl)amino)propanoate (47375-32-6) + p-Cumaldehyd-phenylsulfonylhydrazon (50626-30-7) → (S)-methyl 2-(((benzyloxy)carbonyl)amino)-3-(4-(5-(4-isopropylphenyl)-2H-tetrazol-2-yl)phenyl)propanoate

Guidance literature:

(S)-methyl 3-(4-aminophenyl)-2-(((benzyloxy)carbonyl)amino)propanoate; With hydrogenchloride; sodium nitrite; In ethanol; water; at -5 - 0 ℃;

p-Cumaldehyd-phenylsulfonylhydrazon; With pyridine; In ethanol; water; at -20 - 20 ℃;

DOI:10.1016/j.bmc.2015.03.006

upstream raw materials:

(4-isopropylbenzaldehyde)

benzenesufonyl hydrazide