C₄₆H₄₆N₂O₈S₂

Base Information

Chemical Name:C₄₆H₄₆N₂O₈S₂
CAS No.:1262795-78-7
Molecular Formula:C₄₆H₄₆N₂O₈S₂
Molecular Weight:819.012
Hs Code.:

C<sub>46</sub>H<sub>46</sub>N<sub>2</sub>O<sub>8</sub>S<sub>2</sub>

Synonyms:C₄₆H₄₆N₂O₈S₂

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Chemical Property of C₄₆H₄₆N₂O₈S₂

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Technology Process of C₄₆H₄₆N₂O₈S₂

There total 7 articles about C₄₆H₄₆N₂O₈S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1262795-64-1
C₂₃H₂₃NO₄S

: C₂₃H₂₃NO₄S

: 1262795-78-7
C₄₆H₄₆N₂O₈S₂

Guidance literature:: With N,N'-bis(benzyliden)ethylendiamine; palladium(II) acetate; In 1,2-dichloro-ethane; at 56 ℃; for 2h; Inert atmosphere;
DOI:10.1071/CH10359

Reference yield:

: 1262795-58-3
C₁₁H₁₈BrNO₂

: C₂₃H₂₃NO₄S

: 1262795-78-7
C₄₆H₄₆N₂O₈S₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: trifluoroacetic acid / dichloromethane / 2.5 h / 18 °C / Inert atmosphere

2.1: dmap; triethylamine / dichloromethane / 1 h / 18 °C / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; benzene / 5 h / 80 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

4.2: 3.5 h / 0 - 18 °C / Inert atmosphere

5.1: palladium(II) acetate; N,N'-bis(benzyliden)ethylendiamine / 1,2-dichloro-ethane / 2 h / 56 °C / Inert atmosphere

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N'-bis(benzyliden)ethylendiamine; palladium(II) acetate; sodium hydride; sodium carbonate; triethylamine; trifluoroacetic acid; In ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil; benzene; 3.1: Suzuki coupling;
DOI:10.1071/CH10359

Reference yield:

: 1262795-59-4
C₁₃H₁₆BrNO₂S

: C₂₃H₂₃NO₄S

: 1262795-78-7
C₄₆H₄₆N₂O₈S₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; benzene / 5 h / 80 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

2.2: 3.5 h / 0 - 18 °C / Inert atmosphere

3.1: palladium(II) acetate; N,N'-bis(benzyliden)ethylendiamine / 1,2-dichloro-ethane / 2 h / 56 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N'-bis(benzyliden)ethylendiamine; palladium(II) acetate; sodium hydride; sodium carbonate; In ethanol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil; benzene; 1.1: Suzuki coupling;
DOI:10.1071/CH10359