1-Benzyloxycarbonyl-4t,5t-O-(isopropyliden)hexahydropyridazin-3r-carbaldehyd-dimethylacetal

Base Information

Chemical Name:1-Benzyloxycarbonyl-4t,5t-O-(isopropyliden)hexahydropyridazin-3r-carbaldehyd-dimethylacetal
CAS No.:75773-34-1
Molecular Formula:C₁₈H₂₆N₂O₆
Molecular Weight:366.414
Hs Code.:

Synonyms:1-Benzyloxycarbonyl-4t,5t-O-(isopropyliden)hexahydropyridazin-3r-carbaldehyd-dimethylacetal

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Chemical Property of 1-Benzyloxycarbonyl-4t,5t-O-(isopropyliden)hexahydropyridazin-3r-carbaldehyd-dimethylacetal

Chemical Property:

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Technology Process of 1-Benzyloxycarbonyl-4t,5t-O-(isopropyliden)hexahydropyridazin-3r-carbaldehyd-dimethylacetal

There total 5 articles about 1-Benzyloxycarbonyl-4t,5t-O-(isopropyliden)hexahydropyridazin-3r-carbaldehyd-dimethylacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75773-30-7
3r-Dimethoxymethyl-4t,5t-O-isopropyliden-3,4,5,6-tetrahydropyridazin-1,2-dicarbonsaeure-dibenzylester

: 75773-35-2
4t,5t-O-(Isopropyliden)hexahydropyridazin-3r-carbaldehyd-dimethylacetal

: 75773-34-1
1-Benzyloxycarbonyl-4t,5t-O-(isopropyliden)hexahydropyridazin-3r-carbaldehyd-dimethylacetal

Guidance literature:: With hydrogen; palladium; In methanol; for 80h;

Reference yield:

: 20432-40-0
(E)-penta-2,4-dienal

: 75773-34-1
1-Benzyloxycarbonyl-4t,5t-O-(isopropyliden)hexahydropyridazin-3r-carbaldehyd-dimethylacetal

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent

2: 67 percent / CH₂Cl₂ / 24 h / Ambient temperature

3: 16 percent / KMnO₄/H₂O / methanol / 1 h / Ambient temperature

4: 91 percent / Bis(p-nitrophenyl)phosphat / various solvent(s) / 1.5 h / Ambient temperature

5: 46 percent / H₂ / Pd / methanol / 80 h

With potassium permanganate; Bis(p-nitrophenyl) phosphate; water; hydrogen; palladium; In methanol; dichloromethane;

Reference yield:

: 75773-20-5
3-Dimethoxymethyl-3,6-dihydropyridazin-1,2-dicarbonsaeure-dibenzylester

: 75773-34-1
1-Benzyloxycarbonyl-4t,5t-O-(isopropyliden)hexahydropyridazin-3r-carbaldehyd-dimethylacetal

Guidance literature:: Multi-step reaction with 3 steps

1: 16 percent / KMnO₄/H₂O / methanol / 1 h / Ambient temperature

2: 91 percent / Bis(p-nitrophenyl)phosphat / various solvent(s) / 1.5 h / Ambient temperature

3: 46 percent / H₂ / Pd / methanol / 80 h

With potassium permanganate; Bis(p-nitrophenyl) phosphate; water; hydrogen; palladium; In methanol;