3r-Dimethoxymethyl-4t,5t-O-isopropyliden-3,4,5,6-tetrahydropyridazin-1,2-dicarbonsaeure-dibenzylester

Base Information

Chemical Name:3r-Dimethoxymethyl-4t,5t-O-isopropyliden-3,4,5,6-tetrahydropyridazin-1,2-dicarbonsaeure-dibenzylester
CAS No.:75773-30-7
Molecular Formula:C₂₆H₃₂N₂O₈
Molecular Weight:500.549
Hs Code.:

Synonyms:3r-Dimethoxymethyl-4t,5t-O-isopropyliden-3,4,5,6-tetrahydropyridazin-1,2-dicarbonsaeure-dibenzylester

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Chemical Property of 3r-Dimethoxymethyl-4t,5t-O-isopropyliden-3,4,5,6-tetrahydropyridazin-1,2-dicarbonsaeure-dibenzylester

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Technology Process of 3r-Dimethoxymethyl-4t,5t-O-isopropyliden-3,4,5,6-tetrahydropyridazin-1,2-dicarbonsaeure-dibenzylester

There total 4 articles about 3r-Dimethoxymethyl-4t,5t-O-isopropyliden-3,4,5,6-tetrahydropyridazin-1,2-dicarbonsaeure-dibenzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 75773-27-2
3r-Dimethoxymethyl-4t,5t-dihydroxy-3,4,5,6-tetrahydropyridazin-1,2-dicarbonsaeure-dibenzylester

: 67-64-1
acetone

: 75773-30-7
3r-Dimethoxymethyl-4t,5t-O-isopropyliden-3,4,5,6-tetrahydropyridazin-1,2-dicarbonsaeure-dibenzylester

Guidance literature:: With Bis(p-nitrophenyl) phosphate; In various solvent(s); for 1.5h; Ambient temperature;

Reference yield:

: 20432-40-0
(E)-penta-2,4-dienal

: 75773-30-7
3r-Dimethoxymethyl-4t,5t-O-isopropyliden-3,4,5,6-tetrahydropyridazin-1,2-dicarbonsaeure-dibenzylester

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent

2: 67 percent / CH₂Cl₂ / 24 h / Ambient temperature

3: 16 percent / KMnO₄/H₂O / methanol / 1 h / Ambient temperature

4: 91 percent / Bis(p-nitrophenyl)phosphat / various solvent(s) / 1.5 h / Ambient temperature

With potassium permanganate; Bis(p-nitrophenyl) phosphate; water; In methanol; dichloromethane;

Reference yield:

: 75773-20-5
3-Dimethoxymethyl-3,6-dihydropyridazin-1,2-dicarbonsaeure-dibenzylester

: 75773-30-7
3r-Dimethoxymethyl-4t,5t-O-isopropyliden-3,4,5,6-tetrahydropyridazin-1,2-dicarbonsaeure-dibenzylester

Guidance literature:: Multi-step reaction with 2 steps

1: 16 percent / KMnO₄/H₂O / methanol / 1 h / Ambient temperature

2: 91 percent / Bis(p-nitrophenyl)phosphat / various solvent(s) / 1.5 h / Ambient temperature

With potassium permanganate; Bis(p-nitrophenyl) phosphate; water; In methanol;