3-(4-acetyl-5-methyl-1-(p-tolyl)-1H-pyrazol-3-carbonyl)-1,5-diphenyl-1H-pyrazole-4-carbonitrile

Base Information

• Chemical Name: 3-(4-acetyl-5-methyl-1-(p-tolyl)-1H-pyrazol-3-carbonyl)-1,5-diphenyl-1H-pyrazole-4-carbonitrile
• CAS No.: 1227951-84-9
• Molecular Formula: C₃₀H₂₃N₅O₂
• Molecular Weight: 485.545

Synonyms:3-(4-acetyl-5-methyl-1-(p-tolyl)-1H-pyrazol-3-carbonyl)-1,5-diphenyl-1H-pyrazole-4-carbonitrile

Chemical Property of 3-(4-acetyl-5-methyl-1-(p-tolyl)-1H-pyrazol-3-carbonyl)-1,5-diphenyl-1H-pyrazole-4-carbonitrile

Chemical Property:

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Technology Process of 3-(4-acetyl-5-methyl-1-(p-tolyl)-1H-pyrazol-3-carbonyl)-1,5-diphenyl-1H-pyrazole-4-carbonitrile

There total 1 articles about 3-(4-acetyl-5-methyl-1-(p-tolyl)-1H-pyrazol-3-carbonyl)-1,5-diphenyl-1H-pyrazole-4-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

4-cyano-α-oxo-N-(4-tolyl)-1,5-diphenyl-1H-pyrazole-3-ethanehydrazonoyl bromide (1227951-76-9) + acetylacetone (123-54-6,81235-32-7) → 3-(4-acetyl-5-methyl-1-(p-tolyl)-1H-pyrazol-3-carbonyl)-1,5-diphenyl-1H-pyrazole-4-carbonitrile (1227951-84-9)

Guidance literature:

acetylacetone; With sodium ethanolate; In ethanol; for 0.25h;

4-cyano-α-oxo-N-(4-tolyl)-1,5-diphenyl-1H-pyrazole-3-ethanehydrazonoyl bromide; In ethanol; at 20 ℃; for 12h;

DOI:10.3184/030823409X12528547964044

Reference yield: 79.0%

3-(4-acetyl-5-methyl-1-(p-tolyl)-1H-pyrazol-3-carbonyl)-1,5-diphenyl-1H-pyrazole-4-carbonitrile (1227951-84-9) → 7-(4-cyano-1,5-diphenyl-1H-pyrazol-3-yl)-3,4-dimethyl-2-(p-tolyl)-2H-pyrazolo-[3,4-d]-pyridazine (1227951-89-4)

Guidance literature:

With hydrazine hydrate; In ethanol; for 1h; Reflux;

DOI:10.3184/030823409X12528547964044

upstream raw materials:

4-cyano-α-oxo-N-(4-tolyl)-1,5-diphenyl-1H-pyrazole-3-ethanehydrazonoyl bromide

acetylacetone

Downstream raw materials:

7-(4-cyano-1,5-diphenyl-1H-pyrazol-3-yl)-3,4-dimethyl-2-(p-tolyl)-2H-pyrazolo-[3,4-d]-pyridazine

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