2-pyridinesulfenyl bromide

Base Information

• Chemical Name: 2-pyridinesulfenyl bromide
• CAS No.: 66971-99-1
• Molecular Formula: C₅H₄BrNS
• Molecular Weight: 190.063
• Mol file: 66971-99-1.mol

Synonyms:2-pyridinesulfenyl bromide

Chemical Property of 2-pyridinesulfenyl bromide

Chemical Property:

Purity/Quality:

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Technology Process of 2-pyridinesulfenyl bromide

There total 1 articles about 2-pyridinesulfenyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

[Pt(ppy)(η1-S-pyridine-2-thiolate)(PPh3)] + bromine (7726-95-6) → [Pt(2-phenylpyridine)(triphenylphosphine)Br] + 2-pyridinesulfenyl bromide (66971-99-1)

Guidance literature:

In acetone; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c6ra21756g

Reference yield: 90.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 2-pyridinesulfenyl bromide (66971-99-1) → 3-phenyl-2H,3H-[1,3]thiazolo[3,2-a]pyridin-4-ium bromide

Guidance literature:

2-pyridinesulfenyl bromide; With bromine; In chloroform; at 20 ℃; for 0.333333h;

styrene; In chloroform; at 20 ℃; for 6h; regioselective reaction; Reflux;

DOI:10.3390/molecules25020376

Reference yield: 84.0%

1-ethenyl-4-methylbenzene (622-97-9,24936-41-2) + 2-pyridinesulfenyl bromide (66971-99-1) → 3-(4-methylphenyl)-2H,3H-thiazolo[3,2-]pyridin-4-ium bromide

Guidance literature:

2-pyridinesulfenyl bromide; With bromine; In dichloromethane; at 20 ℃; for 0.5h;

1-ethenyl-4-methylbenzene; In dichloromethane; at 20 ℃; for 24h; regioselective reaction;

DOI:10.3390/molecules25020376

upstream raw materials:

bromine

Refernces