C₄₃H₅₅N₅O₁₁

Base Information

Chemical Name:C₄₃H₅₅N₅O₁₁
CAS No.:1334236-88-2
Molecular Formula:C₄₃H₅₅N₅O₁₁
Molecular Weight:817.937
Hs Code.:

C<sub>43</sub>H<sub>55</sub>N<sub>5</sub>O<sub>11</sub>

Synonyms:C₄₃H₅₅N₅O₁₁

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Chemical Property of C₄₃H₅₅N₅O₁₁

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Technology Process of C₄₃H₅₅N₅O₁₁

There total 15 articles about C₄₃H₅₅N₅O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.5%

: 1004524-61-1
C₂₄H₂₉N₃O₆

: 2389-60-8
Z-Lys(Boc)-OH

: 1334236-88-2
C₄₃H₅₅N₅O₁₁

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 30 ℃; for 16h;

Reference yield:

: 94790-24-6
(S)-methyl 2-((tert-butoxycarbonyl)amino)-3-(4-methoxyphenyl)propanoate

: 1334236-88-2
C₄₃H₅₅N₅O₁₁

Guidance literature:: Multi-step reaction with 7 steps

1: silver sulfate; iodine / methanol / 2 h / 20 °C

2: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 3 h / 80 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 20 °C

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide; acetonitrile / 20 °C

5: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium hydrogencarbonate / N,N-dimethyl-formamide / 120 °C / Sealed tube; Inert atmosphere

6: trifluoroacetic acid / dichloromethane

7: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 30 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; iodine; potassium acetate; sodium hydrogencarbonate; benzotriazol-1-ol; silver sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 4326-36-7
(S)-N-(tert-butoxycarbonyl)tyrosine methyl ester

: 1334236-88-2
C₄₃H₅₅N₅O₁₁

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / acetone / 72 h / 20 °C

1.2: 2 h

2.1: silver sulfate; iodine / methanol / 2 h / 20 °C

3.1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 3 h / 80 °C / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane / 20 °C

5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide; acetonitrile / 20 °C

6.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium hydrogencarbonate / N,N-dimethyl-formamide / 120 °C / Sealed tube; Inert atmosphere

7.1: trifluoroacetic acid / dichloromethane

8.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 30 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; iodine; potassium acetate; sodium hydrogencarbonate; potassium carbonate; benzotriazol-1-ol; silver sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; acetonitrile;