2-Chloro-3-fluorophenyl diethylcarbamate

Base Information

Chemical Name:2-Chloro-3-fluorophenyl diethylcarbamate
CAS No.:863870-76-2
Molecular Formula:C11H13 Cl F N O2
Molecular Weight:245.681
Hs Code.:
DSSTox Substance ID:DTXSID10461663
Wikidata:Q82286044
Mol file:863870-76-2.mol

Synonyms:863870-76-2;2-Chloro-3-fluorophenyl diethylcarbamate;(2-chloro-3-fluorophenyl) N,N-diethylcarbamate;2-CHLORO-3-FLUOROPHENYL N,N-DIETHYLCARBAMATE;Carbamic acid,diethyl-, 2-chloro-3-fluorophenyl ester (9CI);2-CHLORO-3-FLUOROPHENYLN,N-DIETHYLCARBAMATE;DTXSID10461663

Suppliers and Price of 2-Chloro-3-fluorophenyl diethylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-CHLORO-3-FLUOROPHENYL N,N-DIETHYLCARBAMATE 95.00%
5MG
$ 495.83

Total 4 raw suppliers

Chemical Property of 2-Chloro-3-fluorophenyl diethylcarbamate

Chemical Property:

PSA：29.54000
LogP:3.31970
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:245.0618845
Heavy Atom Count:16
Complexity:236

Purity/Quality:

97% ^*data from raw suppliers

2-CHLORO-3-FLUOROPHENYL N,N-DIETHYLCARBAMATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=O)OC1=C(C(=CC=C1)F)Cl

Technology Process of 2-Chloro-3-fluorophenyl diethylcarbamate

There total 2 articles about 2-Chloro-3-fluorophenyl diethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 372-20-3
3-fluorophenol

: 863870-76-2
O-2-chloro-3-fluorophenyl N,N-diethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; hexane / -78 - 20 °C

1.2: 89 percent / hexane; tetrahydrofuran / 36 h / Heating

2.1: s-BuLi; TMEDA / cyclohexane; hexane; tetrahydrofuran / 2 h / -78 °C

2.2: 83 percent / hexachloroethane / tetrahydrofuran; hexane; cyclohexane / -78 - 20 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; hexane; cyclohexane;
DOI:10.1021/jo0508402

Reference yield:

: 88-10-8
N,N-diethylcarbamyl chloride

: 863870-76-2
O-2-chloro-3-fluorophenyl N,N-diethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; hexane / -78 - 20 °C

1.2: 89 percent / hexane; tetrahydrofuran / 36 h / Heating

2.1: s-BuLi; TMEDA / cyclohexane; hexane; tetrahydrofuran / 2 h / -78 °C

2.2: 83 percent / hexachloroethane / tetrahydrofuran; hexane; cyclohexane / -78 - 20 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; hexane; cyclohexane;
DOI:10.1021/jo0508402