2-acetamido-6-O-acetyl-3-O-[(R)-1-carboxyethyl]-2-deoxy-α-D-glucopyranoside-1-α-(diphenyl phophate) 1',4-lactone

Base Information

Chemical Name:2-acetamido-6-O-acetyl-3-O-[(R)-1-carboxyethyl]-2-deoxy-α-D-glucopyranoside-1-α-(diphenyl phophate) 1',4-lactone
CAS No.:262853-72-5
Molecular Formula:C₂₅H₂₈NO₁₁P
Molecular Weight:549.471
Hs Code.:

Synonyms:2-acetamido-6-O-acetyl-3-O-[(R)-1-carboxyethyl]-2-deoxy-α-D-glucopyranoside-1-α-(diphenyl phophate) 1',4-lactone

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Chemical Property of 2-acetamido-6-O-acetyl-3-O-[(R)-1-carboxyethyl]-2-deoxy-α-D-glucopyranoside-1-α-(diphenyl phophate) 1',4-lactone

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Technology Process of 2-acetamido-6-O-acetyl-3-O-[(R)-1-carboxyethyl]-2-deoxy-α-D-glucopyranoside-1-α-(diphenyl phophate) 1',4-lactone

There total 2 articles about 2-acetamido-6-O-acetyl-3-O-[(R)-1-carboxyethyl]-2-deoxy-α-D-glucopyranoside-1-α-(diphenyl phophate) 1',4-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 2-acetamido-6-O-acetyl-3-O-[(R)-1-carboxyethyl]-2-deoxy-D-glucopyranoside 1',4-lactone

: 262853-72-5
2-acetamido-6-O-acetyl-3-O-[(R)-1-carboxyethyl]-2-deoxy-α-D-glucopyranoside-1-α-(diphenyl phophate) 1',4-lactone

Guidance literature:: 4-pyrrolidin-1-ylpyridine; In dichloromethane; at -30 - -25 ℃; for 5h;
DOI:10.1691/ph.2008.7675

Reference yield:

: 25605-70-3
benzyl 2-acetamido-6-O-acetyl-3-O-<(R)-1-carboxyethyl>-2-deoxy-α-D-glucopyranoside 1',4-lactone

: 262853-72-5
2-acetamido-6-O-acetyl-3-O-[(R)-1-carboxyethyl]-2-deoxy-α-D-glucopyranoside-1-α-(diphenyl phophate) 1',4-lactone

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / H₂ / 10 percent Pd/C / methanol

2: 43 percent / 4-pyrrolidiniopyridine / CH₂Cl₂ / -30 °C

With hydrogen; 4-pyrrolidin-1-ylpyridine; palladium on activated charcoal; In methanol; dichloromethane; 1: Hydrogenolysis / 2: Condensation;
DOI:10.1016/S0960-894X(99)00638-1