thiophosphoric acid O-benzyl ester O'-[2-(bis-{2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-thiophosphoryloxy]-ethyl}-amino)-ethyl] ester O''-(2,2-dimethyl-[1,3]dioxolan-4-ylmethyl) ester

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Chemical Name:thiophosphoric acid O-benzyl ester O'-[2-(bis-{2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-thiophosphoryloxy]-ethyl}-amino)-ethyl] ester O''-(2,2-dimethyl-[1,3]dioxolan-4-ylmethyl) ester
CAS No.:765299-15-8
Molecular Formula:C₄₅H₆₆NO₁₅P₃S₃
Molecular Weight:1050.14
Hs Code.:

thiophosphoric acid <i>O</i>-benzyl ester <i>O</i>'-[2-(bis-{2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-thiophosphoryloxy]-ethyl}-amino)-ethyl] ester <i>O</i>''-(2,2-dimethyl-[1,3]dioxolan-4-ylmethyl) ester

Synonyms:thiophosphoric acid O-benzyl ester O'-[2-(bis-{2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-thiophosphoryloxy]-ethyl}-amino)-ethyl] ester O''-(2,2-dimethyl-[1,3]dioxolan-4-ylmethyl) ester

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Chemical Property of thiophosphoric acid O-benzyl ester O'-[2-(bis-{2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-thiophosphoryloxy]-ethyl}-amino)-ethyl] ester O''-(2,2-dimethyl-[1,3]dioxolan-4-ylmethyl) ester

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Technology Process of thiophosphoric acid O-benzyl ester O'-[2-(bis-{2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-thiophosphoryloxy]-ethyl}-amino)-ethyl] ester O''-(2,2-dimethyl-[1,3]dioxolan-4-ylmethyl) ester

There total 3 articles about thiophosphoric acid O-benzyl ester O'-[2-(bis-{2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-thiophosphoryloxy]-ethyl}-amino)-ethyl] ester O''-(2,2-dimethyl-[1,3]dioxolan-4-ylmethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 765299-13-6
phosphorous acid benzyl ester 2-(bis-{2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphanyloxy]-ethyl}-amino)-ethyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

: 765299-15-8
thiophosphoric acid O-benzyl ester O'-[2-(bis-{2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-thiophosphoryloxy]-ethyl}-amino)-ethyl] ester O''-(2,2-dimethyl-[1,3]dioxolan-4-ylmethyl) ester

Guidance literature:: With sulfur; In toluene; at 20 ℃;
DOI:10.1023/B:RUGC.0000016014.90042.3b

Reference yield:

: 64505-22-2
1,2-O-isopropylideneglycero-3-(benzyldiethylphosphoramidite)

: 765299-15-8
thiophosphoric acid O-benzyl ester O'-[2-(bis-{2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-thiophosphoryloxy]-ethyl}-amino)-ethyl] ester O''-(2,2-dimethyl-[1,3]dioxolan-4-ylmethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: dioxane / 10 h / 90 °C / 500 Torr

2: 0.74 g / sulfur / toluene / 20 °C

With sulfur; In 1,4-dioxane; toluene;
DOI:10.1023/B:RUGC.0000016014.90042.3b

Reference yield:

: 102-71-6,64114-46-1
triethanolamine

: 765299-15-8
thiophosphoric acid O-benzyl ester O'-[2-(bis-{2-[benzyloxy-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-thiophosphoryloxy]-ethyl}-amino)-ethyl] ester O''-(2,2-dimethyl-[1,3]dioxolan-4-ylmethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: dioxane / 10 h / 90 °C / 500 Torr

2: 0.74 g / sulfur / toluene / 20 °C

With sulfur; In 1,4-dioxane; toluene;
DOI:10.1023/B:RUGC.0000016014.90042.3b