4-(3-(2-fluoroethoxy)-2-methoxybenzoyl)-1-piperidinecarboxylic acid t-butyl ester

Base Information

Chemical Name:4-(3-(2-fluoroethoxy)-2-methoxybenzoyl)-1-piperidinecarboxylic acid t-butyl ester
CAS No.:1160298-39-4
Molecular Formula:C₂₀H₂₈FNO₅
Molecular Weight:381.444
Hs Code.:

Synonyms:4-(3-(2-fluoroethoxy)-2-methoxybenzoyl)-1-piperidinecarboxylic acid t-butyl ester

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Chemical Property of 4-(3-(2-fluoroethoxy)-2-methoxybenzoyl)-1-piperidinecarboxylic acid t-butyl ester

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Technology Process of 4-(3-(2-fluoroethoxy)-2-methoxybenzoyl)-1-piperidinecarboxylic acid t-butyl ester

There total 1 articles about 4-(3-(2-fluoroethoxy)-2-methoxybenzoyl)-1-piperidinecarboxylic acid t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 762-49-2
2-fluoroethyl bromide

: 4-(3-hydroxy-2-methoxy-benzoyl)-1-piperidinecarboxylic acid t-butyl ester

: 1160298-39-4
4-(3-(2-fluoroethoxy)-2-methoxybenzoyl)-1-piperidinecarboxylic acid t-butyl ester

Guidance literature:: 4-(3-hydroxy-2-methoxy-benzoyl)-1-piperidinecarboxylic acid t-butyl ester; With sodium hydride; In dimethyl sulfoxide; at 0 ℃;

2-fluoroethyl bromide; In dimethyl sulfoxide; at 60 ℃; for 20h;
DOI:10.1016/j.bmc.2009.03.021

Reference yield: 92.0%

: 1160298-39-4
4-(3-(2-fluoroethoxy)-2-methoxybenzoyl)-1-piperidinecarboxylic acid t-butyl ester

: 1160298-65-6
4-(3-(2-fluoroethoxy)-2-methoxybenzoyl)-piperidine

Guidance literature:: 4-(3-(2-fluoroethoxy)-2-methoxybenzoyl)-1-piperidinecarboxylic acid t-butyl ester; With trifluoroacetic acid; at 20 ℃; for 2h;

With ammonium hydroxide; In diethyl ether; water; Cooling with ice;
DOI:10.1016/j.bmc.2009.03.021