benzyl (2-(1-(2-amino-6-fluorophenyl)piperidin-4-yl)propan-2-yl)carbamate

Base Information

Chemical Name:benzyl (2-(1-(2-amino-6-fluorophenyl)piperidin-4-yl)propan-2-yl)carbamate
CAS No.:1350918-30-7
Molecular Formula:C₂₂H₂₈FN₃O₂
Molecular Weight:385.482
Hs Code.:

Synonyms:benzyl (2-(1-(2-amino-6-fluorophenyl)piperidin-4-yl)propan-2-yl)carbamate

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Chemical Property of benzyl (2-(1-(2-amino-6-fluorophenyl)piperidin-4-yl)propan-2-yl)carbamate

Chemical Property:

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Technology Process of benzyl (2-(1-(2-amino-6-fluorophenyl)piperidin-4-yl)propan-2-yl)carbamate

There total 5 articles about benzyl (2-(1-(2-amino-6-fluorophenyl)piperidin-4-yl)propan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1350918-29-4
benzyl (2-(1-(2-fluoro-6-nitrophenyl)piperidin-4-yl)propan-2-yl)carbamate

: 1350918-30-7
benzyl (2-(1-(2-amino-6-fluorophenyl)piperidin-4-yl)propan-2-yl)carbamate

Guidance literature:: benzyl (2-(1-(2-fluoro-6-nitrophenyl)piperidin-4-yl)propan-2-yl)carbamate; With iron; acetic acid; at 20 ℃;

With sodium hydrogencarbonate; In ethyl acetate; for 0.166667h;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1350918-30-7
benzyl (2-(1-(2-amino-6-fluorophenyl)piperidin-4-yl)propan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / diethyl ether; water / 0 - 25 °C

2.1: trifluoroacetic acid / dichloromethane / 4 h / 25 °C

3.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 80 °C

4.1: acetic acid; iron / 20 °C

4.2: 0.17 h

With iron; potassium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In diethyl ether; dichloromethane; water; acetonitrile;

Reference yield:

: 1057260-89-5
benzyl (2-(piperidin-4-yl)propan-2-yl)carbamate

: 1350918-30-7
benzyl (2-(1-(2-amino-6-fluorophenyl)piperidin-4-yl)propan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 80 °C

2.1: acetic acid; iron / 20 °C

2.2: 0.17 h

With iron; acetic acid; N-ethyl-N,N-diisopropylamine; In acetonitrile;