4-methyl-3-phenyl-5-oxa-1-azatricyclo<6.3.1.0^2,6>dodeca-2(6),3-diene

Base Information

• Chemical Name: 4-methyl-3-phenyl-5-oxa-1-azatricyclo<6.3.1.0^2,6>dodeca-2(6),3-diene
• CAS No.: 50880-50-7
• Molecular Formula: C₁₇H₁₉NO
• Molecular Weight: 253.344
• Mol file: 50880-50-7.mol

Synonyms:4-methyl-3-phenyl-5-oxa-1-azatricyclo<6.3.1.0^2,6>dodeca-2(6),3-diene

Chemical Property of 4-methyl-3-phenyl-5-oxa-1-azatricyclo<6.3.1.0^2,6>dodeca-2(6),3-diene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-methyl-3-phenyl-5-oxa-1-azatricyclo<6.3.1.0^2,6>dodeca-2(6),3-diene

There total 2 articles about 4-methyl-3-phenyl-5-oxa-1-azatricyclo<6.3.1.0^2,6>dodeca-2(6),3-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-(3-phenylprop-2-ynyl)-1-azoniabicyclo<3.3.1>nonan-3-one bromide (50880-48-3) → 4-methyl-3-phenyl-5-oxa-1-azatricyclo<6.3.1.02,6>dodeca-2(6),3-diene (50880-50-7)

Guidance literature:

With sodium hydride; In dimethyl sulfoxide; for 12h; Ambient temperature;

DOI:10.1039/P19810001969

Reference yield: 74.0%

2-(1-phenylpropa-1,2-dienyl)-1-azabicyclo<3.3.1>nonan-3-one (50880-49-4,79841-28-4) → 4-methyl-3-phenyl-5-oxa-1-azatricyclo<6.3.1.02,6>dodeca-2(6),3-diene (50880-50-7)

Guidance literature:

With sodium hydride; In dimethyl sulfoxide; for 4h; Ambient temperature;

DOI:10.1039/P19810001969

upstream raw materials:

1-(3-phenylprop-2-ynyl)-1-azoniabicyclo<3.3.1>nonan-3-one bromide

2-(1-phenylpropa-1,2-dienyl)-1-azabicyclo<3.3.1>nonan-3-one